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Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-

Base Information Edit
  • Chemical Name:Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-
  • CAS No.:396102-32-2
  • Molecular Formula:C17H26O2
  • Molecular Weight:262.392
  • Hs Code.:
  • DSSTox Substance ID:DTXSID60464821
  • Mol file:396102-32-2.mol
Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-

Synonyms:396102-32-2;Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-;DTXSID60464821

Suppliers and Price of Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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  • Chemicals and raw materials
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Total 1 raw suppliers
Chemical Property of Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)- Edit
Chemical Property:
  • XLogP3:5.4
  • Hydrogen Bond Donor Count:0
  • Hydrogen Bond Acceptor Count:2
  • Rotatable Bond Count:3
  • Exact Mass:262.193280068
  • Heavy Atom Count:19
  • Complexity:312
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC1=CC(=C(C(=C1)OC)OC)C2(CCCC2(C)C)C
Technology Process of Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)-

There total 30 articles about Benzene, 1,2-dimethoxy-5-methyl-3-(1,2,2-trimethylcyclopentyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; sodium acetate; platinum(IV) oxide; In acetic acid; at 20 ℃; for 192h; under 1216 - 1368 Torr;
DOI:10.1016/S0040-4020(01)00987-5
Guidance literature:
Multi-step reaction with 14 steps
1.1: NaHCO3; ozone / methanol; CH2Cl2 / 0.22 h / -70 °C
1.2: 80 percent / dimethyl sulfide / methanol; CH2Cl2 / 8 h / 20 °C
2.1: Mg; iodine / diethyl ether
2.2: 88 percent / diethyl ether / 3 h / 20 °C
3.1: 96 percent / PCC; silica gel / CH2Cl2 / 2 h / 20 °C
4.1: sodium hydride / tetrahydrofuran; various solvent(s) / 0.67 h / 20 °C
4.2: tetrahydrofuran; various solvent(s) / 10 h / 20 °C
4.3: 91 percent / tetrahydrofuran; various solvent(s) / 0.5 h / 180 °C
5.1: 90 percent / tetrahydrofuran / 2 h / sonication
6.1: 97 percent / hydrogen / Pd-CaCO3 / ethanol / 24 h / 20 °C
7.1: 85 percent / PCC; silica gel / CH2Cl2 / 30 h / 20 °C
8.1: 75 percent / sodium borohydride / methanol / 1.5 h / cooling
9.1: 28 percent / propionic acid / 48 h / 180 °C
10.1: 80 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / 6 h / 20 °C
11.1: 99 percent / hydrogen / Pd on activated C / ethanol / 3 h / 20 °C / 760 Torr
12.1: 98 percent / LiAlH4 / diethyl ether / 1 h / 0 °C
13.1: 89 percent / PCC; silica gel / CH2Cl2 / 0.5 h / 20 °C
14.1: 77 percent Turnov. / (Ph3P)3RhCl / benzene / 20 h / 120 - 130 °C
With sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; iodine; silica gel; sodium hydride; sodium hydrogencarbonate; ozone; magnesium; propionic acid; pyridinium chlorochromate; palladium on activated charcoal; Wilkinson's catalyst; Grubbs catalyst first generation; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; benzene; 2.2: Grignard reaction / 9.1: Claisen orthoester rearrangement;
DOI:10.1016/j.tet.2006.01.021
Guidance literature:
Multi-step reaction with 11 steps
1.1: sodium hydride / tetrahydrofuran; various solvent(s) / 0.67 h / 20 °C
1.2: tetrahydrofuran; various solvent(s) / 10 h / 20 °C
1.3: 91 percent / tetrahydrofuran; various solvent(s) / 0.5 h / 180 °C
2.1: 90 percent / tetrahydrofuran / 2 h / sonication
3.1: 97 percent / hydrogen / Pd-CaCO3 / ethanol / 24 h / 20 °C
4.1: 85 percent / PCC; silica gel / CH2Cl2 / 30 h / 20 °C
5.1: 75 percent / sodium borohydride / methanol / 1.5 h / cooling
6.1: 28 percent / propionic acid / 48 h / 180 °C
7.1: 80 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / 6 h / 20 °C
8.1: 99 percent / hydrogen / Pd on activated C / ethanol / 3 h / 20 °C / 760 Torr
9.1: 98 percent / LiAlH4 / diethyl ether / 1 h / 0 °C
10.1: 89 percent / PCC; silica gel / CH2Cl2 / 0.5 h / 20 °C
11.1: 77 percent Turnov. / (Ph3P)3RhCl / benzene / 20 h / 120 - 130 °C
With sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; silica gel; sodium hydride; propionic acid; pyridinium chlorochromate; palladium on activated charcoal; Wilkinson's catalyst; Grubbs catalyst first generation; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; benzene; 6.1: Claisen orthoester rearrangement;
DOI:10.1016/j.tet.2006.01.021
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