4-BENZYLOXYANISOLE

Base Information

• Chemical Name: 4-BENZYLOXYANISOLE
• CAS No.: 6630-18-8
• Molecular Formula: C14H14O2
• Molecular Weight: 214.264
• Hs Code.: 2909309090
• Mol file: 6630-18-8.mol

Synonyms:Benzene,1-(benzyloxy)-4-methoxy- (6CI,7CI);Ether, benzyl p-methoxyphenyl (8CI);1-(Benzyloxy)-4-methoxybenzene;1-Methoxy-4-(phenylmethoxy)benzene;4-(Benzyloxy)anisole;Benzyl 4-methoxyphenyl ether;Benzyl p-methoxyphenylether;NSC 60031;p-(Benzyloxy)anisole;

Chemical Property of 4-BENZYLOXYANISOLE

Chemical Property:

• Vapor Pressure: 0.000251mmHg at 25°C
• Melting Point: 71 °C
• Refractive Index: 1.56
• Boiling Point: 334.3 °C at 760 mmHg
• Flash Point: 134.9 °C
• PSA: 18.46000
• Density: 1.081 g/cm³
• LogP: 3.27420
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

4-Benzyloxyanisole 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BENZYLOXYANISOLE

There total 33 articles about 4-BENZYLOXYANISOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzyl bromide (100-39-0) + 4-methoxy-phenol (150-76-5) → 4-methoxyphenyl benzyl ether (6630-18-8)

Guidance literature:

With potassium phosphate; tetrabutylammomium bromide; In water; at 20 ℃; for 2h; Sealed tube; Green chemistry;

DOI:10.1016/j.tet.2014.01.004

Reference yield: 99.0%

4-methoxyphenyl acetate (1200-06-2) + benzyl bromide (100-39-0) → 4-methoxyphenyl benzyl ether (6630-18-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1.) 0 deg C, 1 h, 2.) 25 deg C;

Reference yield: 99.0%

1-bromo-4-methoxy-benzene (104-92-7) + benzyl alcohol (100-51-6,185532-71-2) → 4-methoxyphenyl benzyl ether (6630-18-8)

Guidance literature:

With copper(l) iodide; N¹, N²-diphenethyloxalamide; sodium t-butanolate; In 1,4-dioxane; for 24h; Schlenk technique; Inert atmosphere; Molecular sieve; Heating;

DOI:10.1021/jacs.8b12142

upstream raw materials:

sodium 4-methoxyphenolate

benzyl chloride

4-methoxyphenyl acetate

benzyl bromide

Downstream raw materials:

4-benzyl-2-methoxyphenol

4-benzyloxy-1-methoxy-2-nitro-benzene

1-benzyloxy-4-methoxy-2-nitro-benzene

N-(4-Methoxyphenyl)-N-phenyl-1-naphthalenemethanamine