1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide

Base Information

Chemical Name:1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide
CAS No.:39922-90-2
Molecular Formula:C14H11NO3S2
Molecular Weight:305.378
Hs Code.:
DSSTox Substance ID:DTXSID10480410
Wikidata:Q82315156
Mol file:39922-90-2.mol

Synonyms:39922-90-2;1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide;DTXSID10480410

Suppliers and Price of 1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:305.01803556
Heavy Atom Count:20
Complexity:477

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)SN2C(=O)C3=CC=CC=C3S2(=O)=O

Technology Process of 1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide

There total 1 articles about 1,2-Benzisothiazol-3(2H)-one, 2-[(4-methylphenyl)thio]-, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 933-00-6
p-methylbenzenesulfenyl chloride

: 81-07-2
saccharin

: 39922-90-2
1,1-dioxo-2-p-tolylsulfanyl-1,2-dihydro-1λ⁶-benzo[d]isothiazol-3-one

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1055/s-1975-23693

Reference yield:

: 39922-90-2
1,1-dioxo-2-p-tolylsulfanyl-1,2-dihydro-1λ⁶-benzo[d]isothiazol-3-one

: N-(4-methyl-2-(4-phenylbut-1-yn-1-yl)phenyl)methanesulfonamide

: N-(4-methyl-2-(2-(p-tolylthio)-3,4-dihydronaphthalen-1-yl)phenyl)methanesulfonamide

: (S)-N-(4-methyl-2-(2-(p-tolylthio)-3,4-dihydronaphthalen-1-yl)phenyl)methanesulfonamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; N-((1S,2S)-2-((2-isopropoxy-6-methylphenyl)thio)-2,3-dihydro-1H-inden-1-yl)-4-methylbenzenesulfonamide; In dichloromethane; chloroform; at -78 ℃; for 18h; enantioselective reaction; Schlenk technique;
DOI:10.1002/anie.201915470

Reference yield:

: 870010-90-5
N-(2-(4-phenylbut-1-yn-1-yl)phenyl)methanesulfonamide

: 39922-90-2
1,1-dioxo-2-p-tolylsulfanyl-1,2-dihydro-1λ⁶-benzo[d]isothiazol-3-one

: N-(2-(2-(p-tolylthio)-3,4-dihydronaphthalen-1-yl)phenyl)methanesulfonamide

: (S)-N-(2-(2-(p-tolylthio)-3,4-dihydronaphthalen-1-yl)phenyl)methanesulfonamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; N-((1S,2S)-2-((2,6-dimethoxyphenyl)selanyl)-2,3-dihydro-1H-inden-1-yl)-1,1,1-trifluoromethanesulfonamide; In dichloromethane; at -78 ℃; for 18h; Overall yield = 37 percentSpectr.; enantioselective reaction; Schlenk technique;
DOI:10.1002/anie.201915470