Aniline, 4,4'-(hexamethylenedioxy)DI-, dihydrochloride

Base Information

• Chemical Name: Aniline, 4,4'-(hexamethylenedioxy)DI-, dihydrochloride
• CAS No.: 6889-02-7
• Molecular Formula: C₁₈H₂₄N₂O₂*2ClH
• Molecular Weight: 373.323
• DSSTox Substance ID: DTXSID30988589
• Mol file: 6889-02-7.mol

Synonyms:ANILINE, 4,4'-(HEXAMETHYLENEDIOXY)DI-, DIHYDROCHLORIDE;6889-02-7;DTXSID30988589;4-[6-(4-aminophenoxy)hexoxy]aniline;dihydrochloride;4,4'-[Hexane-1,6-diylbis(oxy)]dianiline--hydrogen chloride (1/2)

Chemical Property of Aniline, 4,4'-(hexamethylenedioxy)DI-, dihydrochloride

Chemical Property:

• Boiling Point: 518.7°Cat760mmHg
• Flash Point: 289.2°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 372.1371335
• Heavy Atom Count: 24
• Complexity: 244

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1N)OCCCCCCOC2=CC=C(C=C2)N.Cl.Cl

Technology Process of Aniline, 4,4'-(hexamethylenedioxy)DI-, dihydrochloride

There total 3 articles about Aniline, 4,4'-(hexamethylenedioxy)DI-, dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N′-((hexane-1,6-diylbis(oxy))bis(4,1-phenylene))diacetamide (104209-29-2) → 4,4'-<1,6-hexanediylbis(oxy)>bis dihydrochloride (6889-02-7)

Guidance literature:

With hydrogenchloride; In ethanol;

Reference yield:

1 ,6-dibromohexane (629-03-8) → 4,4'-<1,6-hexanediylbis(oxy)>bis dihydrochloride (6889-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: anhydrous K₂CO₃ / dimethylformamide / 4 h / Heating

2: HCl / ethanol

With hydrogenchloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

4-acetaminophenol (103-90-2,8055-08-1) → 4,4'-<1,6-hexanediylbis(oxy)>bis dihydrochloride (6889-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: anhydrous K₂CO₃ / dimethylformamide / 4 h / Heating

2: HCl / ethanol

With hydrogenchloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

N,N′-((hexane-1,6-diylbis(oxy))bis(4,1-phenylene))diacetamide

1 ,6-dibromohexane

4-acetaminophenol

Downstream raw materials:

C₂₈H₄₀N₁₀O₂*2ClH

1,6-bis-(4-aminophenoxy)-hexane