Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI)

Base Information

Chemical Name:Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI)
CAS No.:402822-99-5
Molecular Formula:C12H13NO
Molecular Weight:187.241
Hs Code.:
Mol file:402822-99-5.mol

Synonyms:1-acetyl-4-methyl-1,2-dihydro-quinoline;1-acetyl-4-methyl-1,2-dihydroquinoline;1-Acetyl-4-methyl-1,2-dihydro-chinolin;

Suppliers and Price of Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI)

Chemical Property:

PSA：20.31000
LogP:2.52140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI)

There total 8 articles about Quinoline, 1-acetyl-1,2-dihydro-4-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 402822-95-1
N-allyl-N-acetyl-2-isopropenylaniline

: 402822-99-5
1-(4-methylquinolin-1(2H)-yl)ethanone

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 50 ℃; for 1h;
DOI:10.1016/S0040-4039(01)01714-2

Reference yield:

: 22514-60-9
1,2-dihydrolepidine

: 75-36-5
acetyl chloride

: 402822-99-5
1-(4-methylquinolin-1(2H)-yl)ethanone

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ol401349a

Reference yield:

: 491-35-0
C₆H₄NCH₂CHCCH₂

: 75-36-5
acetyl chloride

: 402822-99-5
1-(4-methylquinolin-1(2H)-yl)ethanone

Guidance literature:: C₆H₄NCH₂CHCCH₂; With chlorobis(cyclooctene)-iridium(I) dimer; H₂SiEt₂; In toluene; at 55 ℃; for 3h;

acetyl chloride;
DOI:10.1039/c6sc01037g