N-[2-(Prop-1-en-2-yl)phenyl]acetamide

Base Information

Chemical Name:N-[2-(Prop-1-en-2-yl)phenyl]acetamide
CAS No.:72934-86-2
Molecular Formula:C11H13NO
Molecular Weight:175.23
Hs Code.:
DSSTox Substance ID:DTXSID80501883
Nikkaji Number:J1.311.325D
Wikidata:Q82354572

Synonyms:72934-86-2;N-[2-(Prop-1-en-2-yl)phenyl]acetamide;N-(2-prop-1-en-2-ylphenyl)acetamide;N-(2-isopropenylphenyl)acetamide;SCHEMBL12074775;DTXSID80501883;AJ-797/43492879

Suppliers and Price of N-[2-(Prop-1-en-2-yl)phenyl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-[2-(Prop-1-en-2-yl)phenyl]acetamide

Chemical Property:

PSA：32.59000
LogP:3.32760
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:175.099714038
Heavy Atom Count:13
Complexity:210

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)C1=CC=CC=C1NC(=O)C

Technology Process of N-[2-(Prop-1-en-2-yl)phenyl]acetamide

There total 8 articles about N-[2-(Prop-1-en-2-yl)phenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52562-19-3
2-isopropenylaniline

: 108-24-7
acetic anhydride

: 72934-86-2
N-[2-(1-methylethenyl)phenyl]acetamide

Guidance literature:: With pyridine;
DOI:10.1246/bcsj.78.886

Reference yield: 88.0%

: 52562-19-3
2-isopropenylaniline

: 75-36-5
acetyl chloride

: 72934-86-2
N-[2-(1-methylethenyl)phenyl]acetamide

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 551-93-9
2-aminoacetophenone

: 72934-86-2
N-[2-(1-methylethenyl)phenyl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

1.2: 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

2.1: triethylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

With potassium tert-butylate; triethylamine; In tetrahydrofuran; dichloromethane; 1.2: |Wittig Olefination;
DOI:10.1039/c5ob01196e