5,6-dimethoxy-1H-1,3-benzodiazol-2-amine

Base Information

Chemical Name:5,6-dimethoxy-1H-1,3-benzodiazol-2-amine
CAS No.:40294-35-7
Molecular Formula:C9H11N3O2
Molecular Weight:193.205
Hs Code.:2933990090
European Community (EC) Number:867-818-5
DSSTox Substance ID:DTXSID001286651
Mol file:40294-35-7.mol

Synonyms:40294-35-7;5,6-dimethoxy-1H-1,3-benzodiazol-2-amine;5,6-Dimethoxy-1H-benzo[d]imidazol-2-amine;5,6-dimethoxy-1H-benzimidazol-2-amine;1H-Benzimidazol-2-amine,5,6-dimethoxy-(9CI);2-amino-5,6-dimethoxybenzimidazole;SCHEMBL9419443;POWPTEBMSHLSRA-UHFFFAOYSA-N;DTXSID001286651;AKOS011973096;CS-0259764;EN300-74169;G57938;Z995046460

Suppliers and Price of 5,6-dimethoxy-1H-1,3-benzodiazol-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5,6-dimethoxy-1H-1,3-benzodiazol-2-amine
100mg
$ 240.00

Alichem
5,6-Dimethoxy-1H-benzo[d]imidazol-2-amine
5g
$ 2150.70

AK Scientific
5,6-Dimethoxy-1H-1,3-benzodiazol-2-amine
10g
$ 2665.00

Total 2 raw suppliers

Chemical Property of 5,6-dimethoxy-1H-1,3-benzodiazol-2-amine

Chemical Property:

PSA：73.89000
LogP:1.09240
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:193.085126602
Heavy Atom Count:14
Complexity:203

Purity/Quality:

99% ^*data from raw suppliers

5,6-dimethoxy-1H-1,3-benzodiazol-2-amine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C(=C1)NC(=N2)N)OC

Technology Process of 5,6-dimethoxy-1H-1,3-benzodiazol-2-amine

There total 5 articles about 5,6-dimethoxy-1H-1,3-benzodiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 506-68-3
bromocyane

: 27841-33-4
4,5-dimethoxybenzene-1,2-diamine

: 40294-35-7
5, 6-dimethoxy-1H-1,3-benzodiazol-2-amine

Guidance literature:: With sodium hydrogencarbonate; In water; at 20 ℃;
DOI:10.1002/jhet.2791

Reference yield:

: 709-09-1
3,4-dimethoxynitrobenzene

: 40294-35-7
5, 6-dimethoxy-1H-1,3-benzodiazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / conc. H₂SO₄, KNO₃ / 0.5 h / -5 - 0 °C

2: H₂ / 10percent Pd/C / methanol / Ambient temperature

3: methanol / 21 h / Ambient temperature

With sulfuric acid; hydrogen; potassium nitrate; palladium on activated charcoal; In methanol;
DOI:10.1016/0223-5234(91)90199-W

Reference yield:

: 3395-03-7
4,5-dimethoxy-1,2-dinitrobenzene

: 40294-35-7
5, 6-dimethoxy-1H-1,3-benzodiazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / Ambient temperature

2: methanol / 21 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/0223-5234(91)90199-W