Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1)
CAS No.:402944-22-3
Molecular Formula:C35H36N2O10.C6H15N
Molecular Weight:745.87
Hs Code.:
Mol file:402944-22-3.mol

Synonyms:

Suppliers and Price of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1)

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1)

There total 3 articles about Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-(hydrogen butanedioate), compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-30-5
succinic acid anhydride

: triethylammonium dihydrogen phosphate

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 402944-22-3
5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-succinate triethylamine salt

Guidance literature:: succinic acid anhydride; 5'-O-(4-4'-dimethoxytrityl)thymidine; With triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

triethylammonium dihydrogen phosphate; In dichloromethane; water;

Reference yield: 100.0%

: 108-30-5
succinic acid anhydride

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 121-44-8
triethylamine

: 402944-22-3
5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-succinate triethylamine salt

Guidance literature:: In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

Reference yield: 90.0%

: 108-30-5
succinic acid anhydride

: 15715-58-9
triethylamine carbonate

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 402944-22-3
5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-succinate triethylamine salt

Guidance literature:: succinic acid anhydride; 5'-O-(4-4'-dimethoxytrityl)thymidine; With pyridine; dmap; In dichloromethane; toluene; at 20 ℃; for 16h;

triethylamine carbonate;