2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)propane-1,3-diol

Base Information

• Chemical Name: 2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)propane-1,3-diol
• CAS No.: 26908-93-0
• Molecular Formula: C₇H₁₀Cl₂N₄O₃
• Molecular Weight: 269.087

Synonyms:1,3-Propanediol,2-[(4,6-dichloro-s-triazin-2-yl)amino]-2-(hydroxymethyl)- (8CI);2-[(4,6-Dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)-1,3-propanediol

Chemical Property of 2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)propane-1,3-diol

Chemical Property:

• Vapor Pressure: 3.33E-16mmHg at 25°C
• Boiling Point: 619.4°Cat760mmHg
• Flash Point: 328.4°C
• Density: 1.741g/cm³

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of 2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)propane-1,3-diol

There total 2 articles about 2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-(hydroxymethyl)propane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2-amino-2-hydroxymethyl-1,3-propanediol (77-86-1) → 2,4-dichloro-6-[1,3-dihydroxy-2-(hydroxymethyl)prop-2-ylamino]-s-triazine (26908-93-0)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at -10 - 20 ℃; for 24h;

DOI:10.1016/j.tet.2008.06.071

Reference yield:

→ 2,4-dichloro-6-[1,3-dihydroxy-2-(hydroxymethyl)prop-2-ylamino]-s-triazine (26908-93-0)

Guidance literature:

Cyanursaeure-chlorid, /BRN= 741883/;

Reference yield:

cis-5(S)-amino-4(S)-(p-nitrophenyl)-1,3-dioxane (161970-50-9) + 2,4-dichloro-6-[1,3-dihydroxy-2-(hydroxymethyl)prop-2-ylamino]-s-triazine (26908-93-0) → 2-chloro-6-{[1,3-dihydroxy-2-(hydroxymethyl)prop-2-yl]amino}-4-{[(4S,5S)-4-(4-nitrophenyl)-1,3-dioxan-5-yl]amino}-s-triazine (1201651-69-5)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 65 ℃; for 12h;

DOI:10.2478/s11532-012-0015-4

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

2-amino-2-hydroxymethyl-1,3-propanediol

Downstream raw materials:

[5-(4,6-Bis-aziridin-1-yl-[1,3,5]triazin-2-ylamino)-2-isopropyl-[1,3]dioxan-5-yl]-methanol

[5-(4,6-Bis-aziridin-1-yl-[1,3,5]triazin-2-ylamino)-2-isopropyl-[1,3]dioxan-5-yl]-methanol

[5-(4,6-Bis-aziridin-1-yl-[1,3,5]triazin-2-ylamino)-2-furan-2-yl-[1,3]dioxan-5-yl]-methanol

2-chloro-6-{[1,3-dihydroxy-2-(hydroxymethyl)prop-2-yl]amino}-4-{[(4S,5S)-4-(4-nitrophenyl)-1,3-dioxan-5-yl]amino}-s-triazine

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