(E)-3-(2-(4-Pyridyl)vinyl)pyridine

Base Information

• Chemical Name: (E)-3-(2-(4-Pyridyl)vinyl)pyridine
• CAS No.: 14802-44-9
• Molecular Formula: C12H10 N2
• Molecular Weight: 182.225
• European Community (EC) Number: 238-867-4,654-447-7
• NSC Number: 61718
• DSSTox Substance ID: DTXSID501277758
• Nikkaji Number: J1.958.605G,J227.195H
• Mol file: 14802-44-9.mol

Synonyms:14802-44-9;(E)-3-(2-(4-Pyridyl)vinyl)pyridine;3-[(E)-2-pyridin-4-ylethenyl]pyridine;(E)-3-[2-(4-PYRIDYL)VINYL]PYRIDINE;Pyridine, 3-[2-(4-pyridinyl)ethenyl]-;EINECS 238-867-4;1-(3-Pyridyl)-2-(4-pyridyl)ethylene;MLS002693342;NSC61718;2682-93-1;SCHEMBL10972532;SCHEMBL10972570;LELJBILQTLAIMQ-ONEGZZNKSA-N;DTXSID501277758;NSC-61718;1-(3-pyridyl)-2-(4-pyridyl)ethene;AKOS025395108;(E)-1-(3-Pyridyl)-2-(4-pyridyl)ethene;3-[(1E)-2-(4-Pyridinyl)ethenyl]pyridine;trans-1-(3-pyridyl)-2-(4-pyridyl)-ethylene;Pyridine, 3-(2-(4-pyridinyl)ethenyl)-, (E)-

Chemical Property of (E)-3-(2-(4-Pyridyl)vinyl)pyridine

Chemical Property:

• Vapor Pressure: 0.000409mmHg at 25°C
• Boiling Point: 326.5°Cat760mmHg
• PKA: 5.31±0.26(Predicted)
• Flash Point: 123.5°C
• PSA: 25.78000
• Density: 1.145g/cm³
• LogP: 2.64700
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 182.084398327
• Heavy Atom Count: 14
• Complexity: 183

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CN=C1)C=CC2=CC=NC=C2
• Isomeric SMILES: C1=CC(=CN=C1)/C=C/C2=CC=NC=C2

Technology Process of (E)-3-(2-(4-Pyridyl)vinyl)pyridine

There total 3 articles about (E)-3-(2-(4-Pyridyl)vinyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-vinylpyridine (100-43-6,329041-72-7) + 3-Bromopyridine (626-55-1,163928-56-1) → trans-1-(pyridin-3-yl)-2-(pyridin-4-yl)ethene (14802-44-9)

Guidance literature:

With potassium carbonate; allylpalladium(II) chloride dimer; Tedicyp; In N,N-dimethyl-formamide; at 140 ℃; for 24h;

DOI:10.1016/S0040-4039(02)01109-7

Reference yield: 65.0%

pyridine (110-86-1) + 4-vinylpyridine (100-43-6,329041-72-7) → trans-1-(pyridin-3-yl)-2-(pyridin-4-yl)ethene (14802-44-9)

Guidance literature:

With N-acetyl-L-valine; oxygen; palladium diacetate; potassium hydrogencarbonate; In tert-Amyl alcohol; at 130 ℃; for 12h; under 760.051 Torr; Schlenk technique; Sealed tube; Inert atmosphere;

DOI:10.1021/om400890p

Reference yield:

4-vinylpyridine (100-43-6,329041-72-7) + 3-iodopyridine (1120-90-7) → trans-1-(pyridin-3-yl)-2-(pyridin-4-yl)ethene (14802-44-9)

Guidance literature:

DOI:10.1039/c7ce00573c

upstream raw materials:

4-vinylpyridine

3-Bromopyridine

pyridine

3-iodopyridine