Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-

Base Information

Chemical Name:Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-
CAS No.:404568-13-4
Molecular Formula:C29H65PSi6
Molecular Weight:613.322
Hs Code.:
DSSTox Substance ID:DTXSID90478517
Nikkaji Number:J1.610.934G
Wikidata:Q82311959

Synonyms:404568-13-4;Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-;DTXSID90478517

Suppliers and Price of Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:612.34394828
Heavy Atom Count:36
Complexity:625

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C(C1=CC(=C(C(=C1)C([Si](C)(C)C)[Si](C)(C)C)P(C)C)C([Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C

Technology Process of Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-

There total 3 articles about Phosphine, dimethyl[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 917-54-4
methyllithium

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 404568-13-4
{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}(dimethyl)phosphine

Guidance literature:: 1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h;

With phosphorus trichloride; In tetrahydrofuran; pentane; at 20 ℃; for 15h;

methyllithium; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃;
DOI:10.1246/bcsj.76.1577

Reference yield:

: 917-54-4
methyllithium

: 125444-10-2
{2,4,6-tris-(bis-(trimethylsilyl)methyl)phenyl}lithium

: 404568-13-4
{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}(dimethyl)phosphine

Guidance literature:: {2,4,6-tris-(bis-(trimethylsilyl)methyl)phenyl}lithium; With phosphorus trichloride; In tetrahydrofuran;

methyllithium; In tetrahydrofuran;
DOI:10.1002/1521-3773(20020104)41:1<136::AID-ANIE136>3.0.CO;2-F