4,5-DIMEIQX

Base Information

Chemical Name:4,5-DIMEIQX
CAS No.:146177-59-5
Molecular Formula:C₁₂H₁₃N₅
Molecular Weight:227.269
Hs Code.:
Mol file:146177-59-5.mol

Synonyms:4,5-DIMEIQX;2-AMINO-3,4,5-TRIMETHYLIMIDAZO(4,5-F)QUINOXALINE

Suppliers and Price of 4,5-DIMEIQX

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4,5-DIMEIQX

Chemical Property:

Vapor Pressure:1.4E-09mmHg at 25°C
Refractive Index:1.6610 (estimate)
Boiling Point:485.5°Cat760mmHg
Flash Point:247.5°C
PSA：70.35000
Density:1.42g/cm³
LogP:1.64560

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,5-DIMEIQX

There total 8 articles about 4,5-DIMEIQX which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 146177-59-5
2-amino-3,4,5-trimethyl-3H-imidazo<4,5-f>quinoxaline

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / pyridinium bromide perbromide, AcOH / 0.5 h / Ambient temperature

2: 87 percent / 25percent aq. NH₃, sodium dithionite / methanol / 3 h / Heating

3: 86 percent / aq. HCl, SeO₂ / 80 °C

4: 69 percent / conc. H₂SO₄, conc. HNO₃ / 1 h / 0 - 20 °C

5: 70 percent / 2-methoxy-ethanol; H₂O / 0.17 h / Heating

6: 40percent aq. NH₄SH / methanol / 3 h / Heating

7: methanol; H₂O / 3 h / Heating

8: H₂ / Raney nickel / aq. ethanol / 1 h / Ambient temperature

9: aq. ethanol / 5 °C

With hydrogenchloride; ammonium hydroxide; selenium(IV) oxide; sodium dithionite; ammonium sulfide; sulfuric acid; hydrogen; nitric acid; pyridinium hydrobromide perbromide; acetic acid; nickel; In methanol; ethanol; 2-methoxy-ethanol; water;

Reference yield:

: 108485-13-8
4-bromo-2,3-dimethyl-6-nitroaniline

: 146177-59-5
2-amino-3,4,5-trimethyl-3H-imidazo<4,5-f>quinoxaline

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / 25percent aq. NH₃, sodium dithionite / methanol / 3 h / Heating

2: 86 percent / aq. HCl, SeO₂ / 80 °C

3: 69 percent / conc. H₂SO₄, conc. HNO₃ / 1 h / 0 - 20 °C

4: 70 percent / 2-methoxy-ethanol; H₂O / 0.17 h / Heating

5: 40percent aq. NH₄SH / methanol / 3 h / Heating

6: methanol; H₂O / 3 h / Heating

7: H₂ / Raney nickel / aq. ethanol / 1 h / Ambient temperature

8: aq. ethanol / 5 °C

With hydrogenchloride; ammonium hydroxide; selenium(IV) oxide; sodium dithionite; ammonium sulfide; sulfuric acid; hydrogen; nitric acid; nickel; In methanol; ethanol; 2-methoxy-ethanol; water;

Reference yield:

: 107100-16-3
4-bromo-2,3-dimethyl-1,2-benzenediamine

: 146177-59-5
2-amino-3,4,5-trimethyl-3H-imidazo<4,5-f>quinoxaline

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / aq. HCl, SeO₂ / 80 °C

2: 69 percent / conc. H₂SO₄, conc. HNO₃ / 1 h / 0 - 20 °C

3: 70 percent / 2-methoxy-ethanol; H₂O / 0.17 h / Heating

4: 40percent aq. NH₄SH / methanol / 3 h / Heating

5: methanol; H₂O / 3 h / Heating

6: H₂ / Raney nickel / aq. ethanol / 1 h / Ambient temperature

7: aq. ethanol / 5 °C

With hydrogenchloride; selenium(IV) oxide; ammonium sulfide; sulfuric acid; hydrogen; nitric acid; nickel; In methanol; ethanol; 2-methoxy-ethanol; water;