Pyridine-2,6-dialdehyde dioxime

Base Information

• Chemical Name: Pyridine-2,6-dialdehyde dioxime
• CAS No.: 2851-68-5
• Molecular Formula: C7H7 N3 O2
• Molecular Weight: 165.151
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID701270815
• Mol file: 2851-68-5.mol

Synonyms:NCIOpen2_000116;pyridine-2,6-dialdehyde dioxime;SCHEMBL11602459;DTXSID701270815

Chemical Property of Pyridine-2,6-dialdehyde dioxime

Chemical Property:

• Vapor Pressure: 0.002mmHg at 25°C
• Boiling Point: 259.1°Cat760mmHg
• Flash Point: 110.5°C
• PSA: 78.07000
• Density: 1.31g/cm³
• LogP: 0.69780
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 165.053826475
• Heavy Atom Count: 12
• Complexity: 164

Purity/Quality:

99% ^*data from raw suppliers

2,6-Pyridinedicarboxaldehyde2,6-dioxime 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=NC(=C1)C=NO)C=NO

Technology Process of Pyridine-2,6-dialdehyde dioxime

There total 6 articles about Pyridine-2,6-dialdehyde dioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,6-Pyridinedicarboxaldehyde (5431-44-7) → pyridine-2,6-dicarboxaldehyde dioxime (2851-68-5)

Guidance literature:

With hydroxylamine hydrochloride; sodium carbonate; In methanol; at 0 ℃; for 1h;

DOI:10.1055/s-2001-18061

Reference yield:

6-(5-phenyl-isoxazol-3-yl)-pyridine-2-carbaldehyde → pyridine-2,6-dicarboxaldehyde dioxime (2851-68-5)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 1h;

DOI:10.1021/ja0471525

Reference yield:

2,6-Pyridinedicarboxaldehyde (5431-44-7) → pyridine-2,6-dicarbaldehyde dioxime (2851-68-5)

Guidance literature:

upstream raw materials:

2,6-Pyridinedicarboxaldehyde

2,6-dimethylpyridine

6-methyl-2-pyridinecarboxaldehyde

Downstream raw materials:

2,6-bis(aminomethyl)pyridine

2,2'-(pyridine-2,6-diyldimethyldiimino-dimethyl)-bis-phenol