6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide

Base Information

• Chemical Name: 6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide
• CAS No.: 26638-56-2
• Molecular Formula: C₁₄H₁₃NO₃S
• Molecular Weight: 275.328
• Mol file: 26638-56-2.mol

Synonyms:5,11-Dihydro-10,10-dioxo-5-hydroxy-11-methyldibenzo[c,f][1,2]thiazepine

Chemical Property of 6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide

Chemical Property:

• Vapor Pressure: 4.45E-09mmHg at 25°C
• Melting Point: 138-139 °C(Solv: 1-propanol (71-23-8))
• Boiling Point: 455.2°C at 760 mmHg
• PKA: 12.81±0.20(Predicted)
• Flash Point: 229.1°C
• PSA: 65.99000
• Density: 1.387g/cm³
• LogP: 3.05260
• Solubility.: Methanol

Purity/Quality:

97% ^*data from raw suppliers

6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-dioxide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Reagent used in the synthesis of Dibenzo[c,f][1,2]thiazepine derivatives 6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide is a reagent used in the synthesis of Dibenzo[c,f][1,2]thiazepine

Technology Process of 6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide

There total 2 articles about 6,11-Dihydro-6-methyl-dibenzo[c,f][1,2]thiazepin-11-ol 5,5-Dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

6,11-dihydro-6-methyl-5,5,11-trioxo-dibenzo<1,2>thiazepine (26638-46-0) → 6,11-dihydro-11-hydroxy-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide (26638-56-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 3h;

DOI:10.1016/j.bmcl.2007.07.002

Reference yield:

→ 6,11-dihydro-11-hydroxy-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide (26638-56-2)

Guidance literature:

aus entspr. Trioxodibenzothiazepin und NaBH4;

Reference yield: 88.0%

methanol (67-56-1) + 6,11-dihydro-11-hydroxy-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide (26638-56-2) → 6,11-dihydro-11-methoxy-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide (155444-01-2)

Guidance literature:

With hydrogenchloride; 1.) reflux, 3 h, 2.) r.t., overnight;

DOI:10.1002/ardp.19943270306

upstream raw materials:

6,11-dihydro-6-methyl-5,5,11-trioxo-dibenzo<1,2>thiazepine

Downstream raw materials:

6,11-dihydro-11-methoxy-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide

6,11-dihydro-11-(i-propoxy)-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide

6,11-dihydro-11<2-(dimethylamino)ethoxy>-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide, maleate

6,11-dihydro-11<2-(pyrrolidino)ethoxy>-6-methyl-dibenzo<1,2>thiazepine S,S-dioxide, maleate

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