2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine

Base Information

• Chemical Name: 2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine
• CAS No.: 15395-61-6
• Molecular Formula: C13H15 N3
• Molecular Weight: 213.2783
• NSC Number: 176069
• DSSTox Substance ID: DTXSID90306402
• Nikkaji Number: J1.281.593J
• Wikidata: Q82053499

Synonyms:15395-61-6;2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine;NSC176069;SCHEMBL1392847;DTXSID90306402;AKOS000236449;NSC-176069;[2-(pyridin-2-yl)ethyl][(pyridin-2-yl)methyl]amine;2-(Pyridin-2-yl)-N-[(pyridin-2-yl)methyl]ethan-1-amine

Chemical Property of 2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine

Chemical Property:

• Vapor Pressure: 5.72E-05mmHg at 25°C
• Boiling Point: 346.5°Cat760mmHg
• Flash Point: 163.4°C
• Density: 1.095g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 213.126597491
• Heavy Atom Count: 16
• Complexity: 184

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=NC(=C1)CCNCC2=CC=CC=N2

Technology Process of 2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine

There total 11 articles about 2-(Pyridin-2-yl)-N-(pyridin-2-ylmethyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

pyridine-2-carbaldehyde (1121-60-4) + 2-(aminoethyl)pyridine (2706-56-1) → (2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine (15395-61-6)

Guidance literature:

With sodium tetrahydroborate; In methanol;

Reference yield: 73.0%

4-nitro-N-(2-pyridin-2-yl-ethyl)-N-pyridin-2-ylmethyl-benzenesulfonamide (790235-36-8) → (2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine (15395-61-6)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1021/ja050301e

Reference yield: 65.0%

2-vinylpyridine (100-69-6,25014-15-7,27476-03-5,329041-71-6) + 2-(Aminomethyl)pyridine (3731-51-9) → 2-(pyridin-2-yl)-N-(2-(pyridin-2-yl)ethyl)-N-(pyridin-2-ylmethyl)ethan-1-amine (236745-06-5) + (2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine (15395-61-6)

Guidance literature:

With acetic acid; In methanol; at 80 ℃; for 192h; Inert atmosphere;

DOI:10.1021/jacs.7b10529

upstream raw materials:

2-(aminoethyl)pyridine

2-chloromethylpyridine hydrochloride

4-nitro-N-(2-pyridin-2-yl-ethyl)-N-pyridin-2-ylmethyl-benzenesulfonamide

4-nitro-N-(pyridin-2-ylmethyl)benzenesulfonamide

Downstream raw materials:

4-Nitro-2-{[(2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amino]-methyl}-phenol

C₅₁H₄₉N₅O₁₁S

4-bromo-2-(1,4-dimethyl-1,4,7-triazacyclononane-7-ylmethyl)-6-{[N-(2-pyridyl)methyl-N-2-(2-pyridylethyl)amine]-methyl}phenol

C₂₁H₂₃N₅O₂

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