Technology Process of Bellidifolin
There total 7 articles about Bellidifolin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
acetone;
at -5 - 20 ℃;
for 11h;
- Guidance literature:
-
With
sulfuric acid;
at 120 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus pentoxide; methanesulfonic acid / 1.5 h / 80 °C
2: potassium hydroxide; dipotassium peroxodisulfate; pyridine / water / 21 h / 20 °C
3: sodium hydride / acetone / 11 h / -5 - 20 °C
With
pyridine; dipotassium peroxodisulfate; methanesulfonic acid; phosphorus pentoxide; sodium hydride; potassium hydroxide;
In
water; acetone;
