Technology Process of 2,5,8,11,14,17,20-Heptaoxadocosane, 22,22,22-trifluoro-1-phenyl-
There total 3 articles about 2,5,8,11,14,17,20-Heptaoxadocosane, 22,22,22-trifluoro-1-phenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hypochlorite; ruthenium(III) chloride trihydrate / dichloromethane; acetonitrile; water / 1 h / 0 - 20 °C
2.1: sodium hydride / mineral oil; toluene / 0.5 h / 0 °C
2.2: 4 h / 20 °C
2.3: 12 h / 100 °C
With
sodium hypochlorite; ruthenium(III) chloride trihydrate; sodium hydride;
In
dichloromethane; water; toluene; acetonitrile; mineral oil;
DOI:10.1039/C8OB02392A
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thionyl chloride; N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere
2.1: sodium hypochlorite; ruthenium(III) chloride trihydrate / dichloromethane; acetonitrile; water / 1 h / 0 - 20 °C
3.1: sodium hydride / mineral oil; toluene / 0.5 h / 0 °C
3.2: 4 h / 20 °C
3.3: 12 h / 100 °C
With
dmap; sodium hypochlorite; thionyl chloride; ruthenium(III) chloride trihydrate; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water; toluene; acetonitrile; mineral oil;
DOI:10.1039/C8OB02392A
