3-Quinolinecarboxylic acid, 7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-, 2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide

Base Information

Chemical Name:3-Quinolinecarboxylic acid, 7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-, 2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide
CAS No.:406933-11-7
Molecular Formula:C₃₂H₃₂ClN₅O₅
Molecular Weight:602.09
Hs Code.:

3-Quinolinecarboxylic acid,
7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-,
2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide

Synonyms:

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Chemical Property of 3-Quinolinecarboxylic acid, 7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-, 2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide

Chemical Property:

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Technology Process of 3-Quinolinecarboxylic acid, 7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-, 2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide

There total 4 articles about 3-Quinolinecarboxylic acid, 7-chloro-4-hydroxy-2-(1-pyrrolidinylcarbonyl)-, 2-[(1,1-dimethylethoxy)carbonyl]-1-(phenyl-4-pyridinylmethyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 406933-11-7
N'-[7-chloro-4-oxo-2-(pyrrolidine-1-carbonyl)-1,4-dihydro-quinoline-3-carbonyl]-N'-(phenyl-pyridin-4-yl-methyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / tetrahydrofuran

2: H₂ / Pd/C / methanol / 18 h / 2068.59 Torr

3: CMC; DMAP / tetrahydrofuran

With hydrogenchloride; dmap; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00750-9

Reference yield:

: 14548-46-0
4-Benzoylpyridine

: 406933-11-7
N'-[7-chloro-4-oxo-2-(pyrrolidine-1-carbonyl)-1,4-dihydro-quinoline-3-carbonyl]-N'-(phenyl-pyridin-4-yl-methyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / tetrahydrofuran

2: H₂ / Pd/C / methanol / 18 h / 2068.59 Torr

3: CMC; DMAP / tetrahydrofuran

With hydrogenchloride; dmap; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00750-9

Reference yield:

: 109352-73-0
1,1-dimethylethyl (α-4-pyridinylbenzylidene)carbazate

: 406933-11-7
N'-[7-chloro-4-oxo-2-(pyrrolidine-1-carbonyl)-1,4-dihydro-quinoline-3-carbonyl]-N'-(phenyl-pyridin-4-yl-methyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 18 h / 2068.59 Torr

2: CMC; DMAP / tetrahydrofuran

With dmap; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00750-9