2-Butylsuccinic acid dimethyl ester

Base Information

• Chemical Name: 2-Butylsuccinic acid dimethyl ester
• CAS No.: 4136-86-1
• Molecular Formula: C10H18O4
• Molecular Weight: 202.24800
• Hs Code.: 2917190090
• Mol file: 4136-86-1.mol

Synonyms:

Chemical Property of 2-Butylsuccinic acid dimethyl ester

Chemical Property:

• PSA: 52.60000
• LogP: 1.52890

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Butylsuccinic acid dimethyl ester

There total 9 articles about 2-Butylsuccinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C21H20BNO2 + dimethylfumarate (624-49-7) → dimethyl 2-butylsuccinate (4136-86-1)

Guidance literature:

In methanol; acetonitrile; for 14h; Sealed tube; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.1c01996

Reference yield: 80.0%

tetra-n-butyltin(IV) (1461-25-2) + dimethyl cis-but-2-ene-1,4-dioate (624-48-6) → dimethyl 2-butylsuccinate (4136-86-1)

Guidance literature:

With 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; In acetonitrile; Product distribution; Quantum yield; Irradiation; other alkylating agents, sensitizer; electron-transfer-photosensitized conjugate alkylation of alkenes and alkynes; competition experiments, relative efficiency of alkylation; quenching rate constants of different photosensitizers; mechanism;

DOI:10.1021/jo980093r

Reference yield: 31.0%

C22H20BO2(1-)*Li(1+) + dimethylfumarate (624-49-7) → dimethyl 2-butylsuccinate (4136-86-1) + 8,9-dioxa-8a-borabenzo[fg]tetracene

Guidance literature:

In methanol; acetonitrile; at 20 ℃; for 14h; Inert atmosphere; Irradiation; Sealed tube; Glovebox;

DOI:10.1021/jacs.0c04456

upstream raw materials:

methanol

1-hexene

carbon monoxide

n-butylsuccinic acid