2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane

Base Information

• Chemical Name: 2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane
• CAS No.: 21297-72-3
• Molecular Formula: C₁₀H₂₅NO₂Si₂
• Molecular Weight: 247.485
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID7066697
• Nikkaji Number: J422.086B
• Wikidata: Q81993273
• Mol file: 21297-72-3.mol

Synonyms:21297-72-3;2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane;2,2-diethoxy-1-(trimethylsilyl)-1,2-azasilolidine;(2,2-diethoxyazasilolidin-1-yl)-trimethylsilane;1-Aza-2-silacyclopentane, 2,2-diethoxy-1-(trimethylsilyl)-;SCHEMBL906442;DTXSID7066697;1-(trimethyl-silyl)-2,2-diethoxy-1-aza-2-silacyclopentane

Chemical Property of 2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane

Chemical Property:

• Vapor Pressure: 0.0614mmHg at 25°C
• Boiling Point: 231.7°Cat760mmHg
• PKA: 10.87±0.20(Predicted)
• Flash Point: 93.9°C
• PSA: 21.70000
• Density: 0.93g/cm³
• LogP: 2.47680
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 247.14238211
• Heavy Atom Count: 15
• Complexity: 200

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCO[Si]1(CCCN1[Si](C)(C)C)OCC

Technology Process of 2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane

There total 5 articles about 2,2-Diethoxy-1-(trimethylsilyl)-1-aza-2-silacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(3-triethoxysilanyl-propyl)-trimethylsilanyl-amine (21297-73-4) → 2,2-diethoxy-1-trimethylsilyl-1-aza-2-silacyclopentane (21297-72-3)

Guidance literature:

With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; for 2h; Reagent/catalyst; Reflux;

DOI:10.1515/mgmc-2018-0005

Reference yield:

chloro-trimethyl-silane (75-77-4) + 3-aminopropyltriethoxysilane (919-30-2,29159-37-3) → 2,2-diethoxy-1-trimethylsilyl-1-aza-2-silacyclopentane (21297-72-3)

Guidance literature:

With triethylamine; In xylene;

DOI:10.1021/jo01263a119

Reference yield:

N,N-bis(trimethylsilyl)aminopropyltriethoxysilane (17940-89-5) → 2,2-diethoxy-1-trimethylsilyl-1-aza-2-silacyclopentane (21297-72-3)

Guidance literature:

With ammonium sulfate;

DOI:10.1021/jo01263a119

upstream raw materials:

chloro-trimethyl-silane

3-aminopropyltriethoxysilane

N,N-bis(trimethylsilyl)aminopropyltriethoxysilane

(3-triethoxysilanyl-propyl)-trimethylsilanyl-amine

Downstream raw materials:

1-pentyl(trimethylsilyl)ether

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