9-Diphenylphosphinylfluorene

Base Information

Chemical Name:9-Diphenylphosphinylfluorene
CAS No.:42328-93-8
Molecular Formula:C25H19OP
Molecular Weight:366.399
Hs Code.:
DSSTox Substance ID:DTXSID901283361
Mol file:42328-93-8.mol

Synonyms:9-diphenylphosphinylfluorene;SCHEMBL13788853;DTXSID901283361;9H-Fluoren-9-yldiphenylphosphine oxide;42328-93-8

Suppliers and Price of 9-Diphenylphosphinylfluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 9-Diphenylphosphinylfluorene

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:366.117352223
Heavy Atom Count:27
Complexity:501

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(C2C3=CC=CC=C3C4=CC=CC=C24)C5=CC=CC=C5

Technology Process of 9-Diphenylphosphinylfluorene

There total 6 articles about 9-Diphenylphosphinylfluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 119-61-9
benzophenone

: 4559-70-0
Diphenylphosphine oxide

: 42328-93-8
(9H-fluoren-9-yl)diphenylphosphine oxide

Guidance literature:: With aluminium(III) triflate; trifluoromethylsulfonic anhydride; In toluene; at 120 ℃; for 15h;
DOI:10.1021/acs.orglett.1c02504

Reference yield: 50.0%

: 54458-23-0
diphenyl(9-fluorenyl)phosphine

: 42328-93-8
(9H-fluoren-9-yl)diphenylphosphine oxide

Guidance literature:: With oxygen; In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1080/10426500390228639

Reference yield: 44.0%

: C₁₆H₁₈N⁽¹⁺⁾*CF₃O₃S^(1-)

: 4559-70-0
Diphenylphosphine oxide

: 42328-93-8
(9H-fluoren-9-yl)diphenylphosphine oxide

Guidance literature:: With 18-crown-6 ether; potassium tert-butylate; at 60 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c02992