Technology Process of Phenol, 4-hexyl-2-methoxy-
There total 5 articles about Phenol, 4-hexyl-2-methoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethanol;
for 6h;
under 760.051 Torr;
DOI:10.1002/cmdc.201300429
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pentyltriphenylphosphonium bromide / cyclohexane; tetrahydrofuran / 0.5 h / -78 °C
1.2: 2 h / Cooling
2.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr
With
palladium on activated charcoal; pentyltriphenylphosphonium bromide; hydrogen;
In
tetrahydrofuran; ethanol; cyclohexane;
DOI:10.1002/cmdc.201300429
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / methanol; water / 2 h / Reflux
2.1: pentyltriphenylphosphonium bromide / cyclohexane; tetrahydrofuran / 0.5 h / -78 °C
2.2: 2 h / Cooling
3.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr
With
palladium on activated charcoal; pentyltriphenylphosphonium bromide; hydrogen; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; cyclohexane; water;
DOI:10.1002/cmdc.201300429