3-Methyl-4-methylidenecyclohex-2-en-1-one

Base Information

Chemical Name:3-Methyl-4-methylidenecyclohex-2-en-1-one
CAS No.:42723-25-1
Molecular Formula:C8H10O
Molecular Weight:122.167
Hs Code.:
DSSTox Substance ID:DTXSID10501295
Nikkaji Number:J3.077.421C
Wikidata:Q82353586
Mol file:42723-25-1.mol

Synonyms:3-methyl-4-methylidenecyclohex-2-en-1-one;42723-25-1;SCHEMBL11715124;DTXSID10501295

Suppliers and Price of 3-Methyl-4-methylidenecyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Methyl-4-methylidenecyclohex-2-en-1-one

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:122.073164938
Heavy Atom Count:9
Complexity:187

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=O)CCC1=C

Technology Process of 3-Methyl-4-methylidenecyclohex-2-en-1-one

There total 7 articles about 3-Methyl-4-methylidenecyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 32917-26-3
ethyl 4,4-(ethylenedioxy)-2-methylcyclohex-1-ene-1-carboxylate

: 3-methylcyclohex-3-enone-4-hydroxylmethyl ethyleneketal

: 42723-25-1
3-methyl-4-methylenecyclohex-2-enone

Guidance literature:: With hydrogenchloride; sodium hydroxide; nitrogen; In tetrahydrofuran;

Reference yield:

: 78-94-4,25038-87-3
methyl vinyl ketone

: 22289-05-0
3-methyleneheptane-2,6-dione

: 42723-25-1
3-methyl-4-methylenecyclohex-2-enone

Guidance literature:: tris(N,N-dimethylaminomethyl)phosphine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1002/adsc.200700071

Reference yield:

: 32917-26-3
ethyl 4,4-(ethylenedioxy)-2-methylcyclohex-1-ene-1-carboxylate

: 42723-25-1
3-methyl-4-methylenecyclohex-2-enone

Guidance literature:: With hydrogenchloride; sodium bis(2-methoxyethoxy)aluminium dihydride; Yield given. Multistep reaction; 1.) benzene, THF, room temperature, overnight, 2.) water, room temperature, 4 h;
DOI:10.1021/ja00521a057