2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-

Base Information

Chemical Name:2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-
CAS No.:428857-92-5
Molecular Formula:C14H20O3
Molecular Weight:236.311
Hs Code.:
DSSTox Substance ID:DTXSID80460204
Mol file:428857-92-5.mol

Synonyms:2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-;428857-92-5;DTXSID80460204

Suppliers and Price of 2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:236.14124450
Heavy Atom Count:17
Complexity:188

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCOCCC(COCC1=CC=CC=C1)O

Technology Process of 2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)-

There total 1 articles about 2-Butanol, 1-(phenylmethoxy)-4-(2-propenyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(2-allyloxy-ethyl)-2,2-dibutyl-[1,3,2]dioxastannolane

: 100-39-0
benzyl bromide

: 428857-92-5
(+/-)-4-O-allyl-1-O-benzyl-1,2,4-butanetriol

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 0 ℃; for 12h;
DOI:10.1081/CAR-200050541

Reference yield: 95.0%

: 428857-92-5
(+/-)-4-O-allyl-1-O-benzyl-1,2,4-butanetriol

: 149707-75-5
2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate

: 428857-94-7
4-O-allyl-1-O-benzyl-2-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-butanetriol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1081/CAR-200050541

Reference yield:

: 428857-92-5
(+/-)-4-O-allyl-1-O-benzyl-1,2,4-butanetriol

: 428857-89-0
1-O-benzyl-2-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-butanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / trimethylsilyl trifluoromethanesulfonate; molecular sieves 4 Angstroem / CH₂Cl₂ / 0.17 h / 0 °C

2: 27 percent / acetic acid; sodium acetate; palladium(II) chloride / dioxane / 24 h / 20 °C / pH 4.5

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium acetate; acetic acid; palladium dichloride; In 1,4-dioxane; dichloromethane;
DOI:10.1081/CAR-200050541