Benzenecarboximidothioic acid, N-phenyl-, phenyl ester

Base Information

• Chemical Name: Benzenecarboximidothioic acid, N-phenyl-, phenyl ester
• CAS No.: 4494-63-7
• Molecular Formula: C19H15NS
• Molecular Weight: 289.401

Synonyms:

Chemical Property of Benzenecarboximidothioic acid, N-phenyl-, phenyl ester

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

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Technology Process of Benzenecarboximidothioic acid, N-phenyl-, phenyl ester

There total 6 articles about Benzenecarboximidothioic acid, N-phenyl-, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N,N'-diphenyl-1,2-diphenylethane-1,2-diimine (7510-33-0) + 2,4-bis(phenylthio)-1,3-dithia-2λ5,4λ5-diphosphetane 2,4-disulphide (60118-15-2,95591-54-1) → phenyl-(phenylthio)--methane (4494-63-7)

Guidance literature:

In toluene; for 0.666667h; Mechanism; Heating; other benzil dianiles;

Reference yield: 55.0%

benzenediazonium tetrafluoroborate (369-57-3) + N-Phenylbenzothioamide (636-04-4) → phenyl-(phenylthio)--methane (4494-63-7)

Guidance literature:

With ferrocene; In acetone; for 1.5h;

Reference yield:

N-phenyl-benzimidoyl chloride (4903-36-0) + para-thiocresol (106-45-6) → C20H17NS + N-Phenyl-thiobenzimidic acid phenyl ester (4494-63-7,97563-72-9)

Guidance literature:

With triethylamine; In benzene; for 3h; optical yield given as %de; Reflux;

DOI:10.1021/ol101289k

upstream raw materials:

sodium thiophenolate

N-phenyl-benzimidoyl chloride

N,N'-diphenyl-1,2-diphenylethane-1,2-diimine

2,4-bis(phenylthio)-1,3-dithia-2λ⁵,4λ⁵-diphosphetane 2,4-disulphide

Downstream raw materials:

2-Phenylbenzothiazole

diphenyl sulfide

thiophenol

benzonitrile

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