2'-Allyl-3',4'-dimethoxyacetophenone

Base Information

Chemical Name:2'-Allyl-3',4'-dimethoxyacetophenone
CAS No.:469898-40-6
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:
DSSTox Substance ID:DTXSID201235478
Nikkaji Number:J1.726.465F

Synonyms:DTXSID201235478;2'-Allyl-3',4'-dimethoxyacetophenone;1-[3,4-Dimethoxy-2-(2-propen-1-yl)phenyl]ethanone;469898-40-6

Suppliers and Price of 2'-Allyl-3',4'-dimethoxyacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2'-Allyl-3',4'-dimethoxyacetophenone

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:220.109944368
Heavy Atom Count:16
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=C(C(=C(C=C1)OC)OC)CC=C

Technology Process of 2'-Allyl-3',4'-dimethoxyacetophenone

There total 9 articles about 2'-Allyl-3',4'-dimethoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24002-85-5
4-acetyl-3-allyl-2-hydroxy-1-methoxybenzene

: 74-88-4
methyl iodide

: 469898-40-6
1-(2-allyl-3,4-dimethoxy-phenyl)-ethanone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.03.016

Reference yield: 82.0%

: 469898-63-3
3,4-dimethoxy-1-(1'-hydroxyethyl)-2-(prop-2'-enyl)benzene

: 469898-40-6
1-(2-allyl-3,4-dimethoxy-phenyl)-ethanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/acs.orglett.7b00630

Reference yield:

: 18075-41-7
2-allyl-3-hydroxy-4-methoxybenzaldehyde

: 469898-40-6
1-(2-allyl-3,4-dimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 6.64 g / potassium carbonate / dimethylformamide / 24 h / 80 °C

2: 93 percent / diethyl ether / 0.67 h / 20 °C

3: 57 percent / activated manganese dioxide / benzene / 0.67 h / Heating

With manganese(IV) oxide; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(03)00328-4