Chloroformic acid p-menthan-3-yl ester

Base Information

• Chemical Name: Chloroformic acid p-menthan-3-yl ester
• CAS No.: 50277-59-3
• Molecular Formula: C11H19ClO2
• Molecular Weight: 218.724
• Hs Code.: 2915900090
• Mol file: 50277-59-3.mol

Synonyms:1-menthyloxycarbonyl chloride;chlorocarbonic acid menthyl ester;menthane-3-yl chloroformate;Chlorokohlensaeure-menthylester;menthyl chloroformate;(-) menthylchloroformate;

Chemical Property of Chloroformic acid p-menthan-3-yl ester

Chemical Property:

• PSA: 26.30000
• LogP: 3.82260

Purity/Quality:

97% ^*data from raw suppliers

2-Isopropyl-5-methylcyclohexylcarbonochloridate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Chloroformic acid p-menthan-3-yl ester

There total 4 articles about Chloroformic acid p-menthan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + (-)-menthol (2216-51-5) → 2-isopropyl-5-methylcyclohexyl chloroformate (50277-59-3,7635-53-2)

Guidance literature:

With potassium carbonate; benzene;

Reference yield:

bis(trichloromethyl) carbonate (32315-10-9) + menthol (89-78-1) → 2-isopropyl-5-methylcyclohexyl chloroformate (50277-59-3,7635-53-2)

Guidance literature:

With sodium carbonate; In toluene; at 0 ℃; for 6h;

DOI:10.1039/c2pp25091h

Reference yield:

2-isopropyl-5-methylcyclohexyl 2-oxo-2-(pyren-1-yl)ethyl carbonate (1449331-29-6) → 2-isopropyl-5-methylcyclohexyl chloroformate (50277-59-3,7635-53-2)

Guidance literature:

Multi-step reaction with 2 steps

1: water / acetonitrile / pH 7.5 / Photolysis; Inert atmosphere

2: sodium carbonate / toluene / 6 h / 0 °C

With water; sodium carbonate; In toluene; acetonitrile;

DOI:10.1039/c2pp25091h

upstream raw materials:

phosgene

(-)-menthol

bis(trichloromethyl) carbonate

menthol

Downstream raw materials:

2,5-bis(Menthoxycarbonyloxymethylene)-3,6-bis(menthoxycarbonyloxy)-1,4-dioxane

2-hydroxypropyl (2-isopropyl-5-methylcyclohexyl) carbonate

1-hydroxy-2-propyl menthane-3-yl carbonate

(7S,8R,9R)-8-[(+)-Menthyloxycarbonyloxy]-7-(2-methoxyethoxy)-2,3-dimethyl-9-phenyl-7,8,9,10-tetrahydroimidazo[1,2-h][1,7]naphthyridine

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