4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one

Base Information

Chemical Name:4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one
CAS No.:50355-43-6
Molecular Formula:C11H12O3
Molecular Weight:192.214
Hs Code.:
DSSTox Substance ID:DTXSID50707875
Mol file:50355-43-6.mol

Synonyms:4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one;50355-43-6;DTXSID50707875

Suppliers and Price of 4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:192.078644241
Heavy Atom Count:14
Complexity:223

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C=CC1=C(C(=CC=C1)OC)O

Technology Process of 4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one

There total 1 articles about 4-(2-Hydroxy-3-methoxyphenyl)but-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 67-64-1
acetone

: 50355-43-6
4-(2-hydroxy-3-methoxy-phenyl)-but-3-en-2-one

Guidance literature:: With sodium hydroxide; at 25 ℃;
DOI:10.1039/jr9262901578

Reference yield:

: 50355-43-6
4-(2-hydroxy-3-methoxy-phenyl)-but-3-en-2-one

: 1421330-78-0
C₁₁H₁₄N₂O₂

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Reflux;
DOI:10.1016/j.bmcl.2012.11.101

Reference yield:

: 50355-43-6
4-(2-hydroxy-3-methoxy-phenyl)-but-3-en-2-one

: 1421330-85-9
C₁₃H₁₅BrN₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 2 h / Reflux

2: 4-Nitrobenzenesulfonyl chloride; dmap / 2 h / Reflux

With dmap; hydrazine hydrate; 4-Nitrobenzenesulfonyl chloride; In ethanol;
DOI:10.1016/j.bmcl.2012.11.101