n-(3-Methylphenyl)-2-nitrobenzamide

Base Information

Chemical Name:n-(3-Methylphenyl)-2-nitrobenzamide
CAS No.:50623-64-8
Molecular Formula:C14H12N2O3
Molecular Weight:256.261
Hs Code.:
European Community (EC) Number:637-142-3
DSSTox Substance ID:DTXSID90352146
Wikidata:Q82129151
Mol file:50623-64-8.mol

Synonyms:n-(3-methylphenyl)-2-nitrobenzamide;50623-64-8;5246-49-1;2-Nitro-N-(m-tolyl)benzamide;CBMicro_011843;Oprea1_714868;DTXSID90352146;SMSF0005386;MFCD00088434;AKOS001297347;CB15044;LS-08183;BIM-0011848.P001;SR-01000200756;SR-01000200756-1;Z27791047

Suppliers and Price of n-(3-Methylphenyl)-2-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of n-(3-Methylphenyl)-2-nitrobenzamide

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:256.08479225
Heavy Atom Count:19
Complexity:340

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)NC(=O)C2=CC=CC=C2[N+](=O)[O-]

Technology Process of n-(3-Methylphenyl)-2-nitrobenzamide

There total 3 articles about n-(3-Methylphenyl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-44-1
1-amino-3-methylbenzene

: 610-14-0
2-nitrobenzyl chloride

: 50623-64-8
N-(3-methylphenyl)-2-nitrobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm701191z

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 50623-64-8
N-(3-methylphenyl)-2-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / 80 °C / Inert atmosphere

2: pyridine / dichloromethane / 10 h / 20 °C / Inert atmosphere

With pyridine; thionyl chloride; In dichloromethane;
DOI:10.1021/acs.joc.9b02710