2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester

Base Information

• Chemical Name: 2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester
• CAS No.: 5202-32-4
• Molecular Formula: C11H12O8
• DSSTox Substance ID: DTXSID60356631
• Wikidata: Q82136099
• Mol file: 5202-32-4.mol

Synonyms:5202-32-4;2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester;SCHEMBL14720154;DTXSID60356631

Chemical Property of 2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester

Chemical Property:

• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 7
• Exact Mass: 272.05321734
• Heavy Atom Count: 19
• Complexity: 366

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C(=C(O1)C(=O)OC)C(=O)OC)C(=O)OC

Technology Process of 2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester

There total 1 articles about 2,3,4-Furantricarboxylic acid, 5-methoxy-, trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

dimethyl acetylenedicarboxylate (762-42-5) + 2-(2-Oxo-2H-pyran-4-yloxy)-isoindole-1,3-dione (203728-19-2) → 5-methoxy-furan-2,3,4-tricarboxylic acid trimethyl ester (5202-32-4) + 4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxy)-phthalic acid dimethyl ester

Guidance literature:

at 150 ℃; for 20h; Yields of byproduct given;

DOI:10.1039/a708380g

Reference yield:

5-methoxy-furan-2,3,4-tricarboxylic acid trimethyl ester (5202-32-4) → tetramethyl ethylenetetracarboxylate (55525-27-4)

Guidance literature:

With hydrogen; platinum; In acetic acid;

DOI:10.1016/S0040-4039(00)72392-6

upstream raw materials:

dimethyl acetylenedicarboxylate

2-(2-Oxo-2H-pyran-4-yloxy)-isoindole-1,3-dione

Downstream raw materials:

tetramethyl ethylenetetracarboxylate

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