Digermane, 1,1,2,2-tetraethyl-

Base Information

Chemical Name:Digermane, 1,1,2,2-tetraethyl-
CAS No.:52119-02-5
Molecular Formula:C8H22Ge2
Molecular Weight:263.443
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Digermane, 1,1,2,2-tetraethyl-

Chemical Property:

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Technology Process of Digermane, 1,1,2,2-tetraethyl-

There total 3 articles about Digermane, 1,1,2,2-tetraethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.7%

: 6727-87-3
triethylgermyllithium

: 100460-02-4
trimethylsilyldiethylgermane

: 993-84-0
pentaethyldigermane

: 52119-02-5
tetraethyldigermane

: 1188-14-3
Triethylgerman

: 993-62-4
hexaethyldigermane

: 7749-85-1
trimethylsilyltriethylgermane

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; byproducts: Me3SiGeEt2H; Mixt. of Me3SiGeEt2(H) and Et3GeLi in HMPA is stirred for 72 h at 25°C.;
DOI:10.1016/0022-328X(81)80004-6

Reference yield: 15.5%

: 6727-87-3
triethylgermyllithium

: 10177-53-4
diethylchlorogermane

: 993-84-0
pentaethyldigermane

: 52119-02-5
tetraethyldigermane

: 1188-14-3
Triethylgerman

: 993-62-4
hexaethyldigermane

Guidance literature:: With water; In N,N,N,N,N,N-hexamethylphosphoric triamide; To a soln. of Et3GeLi is added Et2Ge(H)Cl at room temp., mixt. is stirred for 1 h (dry Ar).; detected by GLC;;
DOI:10.1016/0022-328X(81)80004-6

Reference yield: 11.0%

: 993-84-0
pentaethyldigermane

: 110-05-4
di-tert-butyl peroxide

: 52119-02-5
tetraethyldigermane

: 79411-55-5
((CH₃CH₂)2Ge)4

: 925-90-6
ethylmagnesium bromide

: 13937-05-8
octaethyltrigermane

Guidance literature:: In benzene; Irradiation (UV/VIS); digermane soln. irradiating in the presence of an excess of t-Bu2O2; product content detd. by high-pressure chromy.;
DOI:10.1016/0022-328X(84)85145-1