CID 4154598

Base Information

Chemical Name:CID 4154598
CAS No.:20909-39-1
Molecular Formula:C32H16 N8 Pd
Molecular Weight:618.953
Hs Code.:
Mol file:20909-39-1.mol

Synonyms:AKOS002375072

Suppliers and Price of CID 4154598

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 15 raw suppliers

Chemical Property of CID 4154598

Chemical Property:

Melting Point:>360 °C
Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：84.02000
Density:g/cm³
LogP:1.46440
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:618.05327
Heavy Atom Count:41
Complexity:1080

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: S22:Do not inhale dust.; S24/25:Avoid contact with skin and eyes.;

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=NC4=NC(=NC5=C6C=CC=CC6=C([N-]5)N=C7C8=CC=CC=C8C(=N7)N=C2[N-]3)C9=CC=CC=C94.[Pd+2]

Technology Process of CID 4154598

There total 7 articles about CID 4154598 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 85-44-9
phthalic anhydride

: palladium dichloride

: 20909-39-1
palladium(II) phthalocyanine

Guidance literature:: With ammonium chloride; urea; ammonium molybdate; In solid; other Radiation; ligand, urea, NH4Cl, (NH4)2MoO4 and PdCl2 were finely ground, placed in beaker and irradiated in microwave oven at high power for 4 min, oven power turned to medium, 2 min; ground, washed with hot water, dried, repptd. from conc. H2SO4, soxhlet extn. for 3 h with acetone; elem. anal.;

Reference yield: 68.0%

: 136918-14-4,85-41-6
phthalimide

: 57-13-6
urea

: palladium dichloride

: 20909-39-1
palladium(II) phthalocyanine

Guidance literature:: ammonium molybdate; In nitrobenzene; PdCl2, phtalimide, and urea are heated in boiling nitrobenzene for 4 h in the presence of ammonium molybdate as catalyst, greasy impurities are formed.; Washing in succession with isopropanol, 2-3% NaOH, and 2-3% HCl, recrystn. (dissolving in concd. H2SO4, pptn. by addn. of dilute H2SO4), Soxhlet extn. (py/H2O, methanol, acetone), elem. anal..;

Reference yield: 60.0%

: 91-15-6
phthalonitrile

: palladium dichloride

: 20909-39-1
palladium(II) phthalocyanine

Guidance literature:: With 1,8-diazabicyclo{5.4.0}undec-7-ene; In ethanol; byproducts: H2Pc; always conatminated with metal-free phthalocyanine;;
DOI:10.1246/cl.1983.313