Benzene, 1,2,5-trimethoxy-3-(2-propenyl)-

Base Information

Chemical Name:Benzene, 1,2,5-trimethoxy-3-(2-propenyl)-
CAS No.:5273-91-6
Molecular Formula:C12H16O3
Molecular Weight:208.257
Hs Code.:
Mol file:5273-91-6.mol

Synonyms:1-Allyl-2,3,5-trimethoxy-benzene;2,3,5-Trimethoxy-1-allyl-benzol;2,4-dimethoxy-6-allylanisole;2,3,5-trimethoxyallylbenzene;1,2,5-trimethoxy-3-allylbenzene;

Suppliers and Price of Benzene, 1,2,5-trimethoxy-3-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzene, 1,2,5-trimethoxy-3-(2-propenyl)-

Chemical Property:

PSA：27.69000
LogP:2.44090

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, 1,2,5-trimethoxy-3-(2-propenyl)-

There total 8 articles about Benzene, 1,2,5-trimethoxy-3-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 77-78-1
dimethyl sulfate

: 31788-39-3
2-methoxy-6-prop-2'-enylbenzene-1,4-diol

: 5273-91-6
1,3,5-trimethoxy-3-prop-2-enylbenzene

Guidance literature:: With potassium hydroxide; In water; at 80 ℃; for 1h;

Reference yield: 43.0%

: 100612-87-1
1-(2-allyl-3-hydroxy-4,6-dimethoxyphenyl)ethanone

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 5273-91-6
1,3,5-trimethoxy-3-prop-2-enylbenzene

Guidance literature:: With potassium carbonate; In acetone; for 16h; Reflux;
DOI:10.1039/b916372g

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 5273-91-6
1,3,5-trimethoxy-3-prop-2-enylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone / 2 h / Heating

2: 8 h / 185 °C

3: 3percent aq. H₂O₂ / 24 h

4: 2 g / 10percent aq. KOH / 1 h / 80 °C

With potassium carbonate; In acetone; 1: Etherification / 2: Claisen rearrangement / 3: Dakin reaction / 4: Methylation;
DOI:10.1021/jm000905n