2,4,6-trimethylbenzo[h]quinoline

Base Information

Chemical Name:2,4,6-trimethylbenzo[h]quinoline
CAS No.:81503-62-0
Molecular Formula:C₁₆H₁₅N
Molecular Weight:221.302
Hs Code.:

Synonyms:

Suppliers and Price of 2,4,6-trimethylbenzo[h]quinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,4,6-trimethylbenzo[h]quinoline

Chemical Property:

Vapor Pressure:9.48E-06mmHg at 25°C
Boiling Point:383.8°Cat760mmHg
Flash Point:167.8°C
Density:1.108g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6-trimethylbenzo[h]quinoline

There total 4 articles about 2,4,6-trimethylbenzo[h]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4523-45-9
1-amino-4-methylnaphthalene

: 123-54-6,81235-32-7
acetylacetone

: 81503-62-0
2,4,6-trimethylbenzo[h]quinolone

Guidance literature:: With phosphorus pentoxide; silica gel; toluene-4-sulfonic acid; In neat (no solvent); at 155 ℃; for 14h; Inert atmosphere;
DOI:10.1002/cjoc.201700128

Reference yield:

: 880-93-3
4-nitro-1-methylnaphthalene

: 81503-62-0
2,4,6-trimethylbenzo[h]quinolone

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 8 h / 20 °C / 760.05 Torr

2: toluene-4-sulfonic acid; phosphorus pentoxide; silica gel / neat (no solvent) / 14 h / 155 °C / Inert atmosphere

With phosphorus pentoxide; palladium 10% on activated carbon; hydrogen; silica gel; toluene-4-sulfonic acid; In methanol;
DOI:10.1002/cjoc.201700128

Reference yield:

: 90-12-0,34475-76-8
1-Methylnaphthalene

: 81503-62-0
2,4,6-trimethylbenzo[h]quinolone

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / water; ethyl acetate / 0 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 8 h / 20 °C / 760.05 Torr

3: toluene-4-sulfonic acid; phosphorus pentoxide; silica gel / neat (no solvent) / 14 h / 155 °C / Inert atmosphere

With phosphorus pentoxide; palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; toluene-4-sulfonic acid; In methanol; water; ethyl acetate;
DOI:10.1002/cjoc.201700128