1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane

Base Information

• Chemical Name: 1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane
• CAS No.: 53608-84-7
• Molecular Formula: C12H20O2
• Molecular Weight: 196.29
• Hs Code.: 2909209000
• DSSTox Substance ID: DTXSID70446411
• Nikkaji Number: J636.337G
• Wikidata: Q82265041
• Mol file: 53608-84-7.mol

Synonyms:53608-84-7;1,1-bis(prop-2-enoxy)cyclohexane;CYCLOHEXANONE DIALLYLACETAL;1,1-diallyloxycyclohexane;1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane;Cyclohexanone diallyl acetal;1,1-bis(allyloxy)cyclohexane;SCHEMBL11303860;DTXSID70446411;Cyclohexanone bis(2-propenyl)acetal;MFCD03425839;AKOS006278911;1,1-BIS(PROP-2-EN-1-YLOXY)CYCLOHEXANE

Chemical Property of 1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane

Chemical Property:

• Boiling Point: 253.5±20.0 °C(Predicted)
• PSA: 18.46000
• Density: 0.92±0.1 g/cm3(Predicted)
• LogP: 3.05200
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 196.146329876
• Heavy Atom Count: 14
• Complexity: 167

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

CYCLOHEXANONE DIALLYLACETAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCOC1(CCCCC1)OCC=C

Technology Process of 1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane

There total 3 articles about 1,1-Bis[(prop-2-en-1-yl)oxy]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

allyloxytrimethylsilane (18146-00-4) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1,1-bis-(2-propenyloxy)-cyclohexane (53608-84-7)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -23 ℃; for 8h;

DOI:10.1080/00397919508011393

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + allyl alcohol (107-18-6) → 1,1-bis-(2-propenyloxy)-cyclohexane (53608-84-7)

Guidance literature:

With toluene-4-sulfonic acid; 2,2-dimethoxy-propane; In hexane;

DOI:10.1021/jo01074a010

Reference yield:

→ 1,1-bis-(2-propenyloxy)-cyclohexane (53608-84-7)

Guidance literature:

/BRN= 1633724/;

upstream raw materials:

cyclohexanone

allyl alcohol

allyloxytrimethylsilane

Downstream raw materials:

2-allylcyclohexan-1-one

1-(2-propen-1-yloxy)cyclohexene

trans-2-allyl-1-cyclohexanol

cis-2-(prop-2-en-1-yl)cyclohexan-1-ol