N-(4-Chlorobenzyl)ethane-1,2-diamine

Base Information

• Chemical Name: N-(4-Chlorobenzyl)ethane-1,2-diamine
• CAS No.: 53654-70-9
• Molecular Formula: C9H13ClN2
• Molecular Weight: 184.669
• Hs Code.: 2921590090
• Mol file: 53654-70-9.mol

Synonyms:(+/-) N-(4-Chlorbenzoyl)valin;N-(4-chloro-benzyl)-ethylenediamine;N-(4-chlorobenzoyl)valine;N-(4-Chlor-benzyl)-aethylendiamin;2-(4-Chloro-benzoylamino)-3-methyl-butyric acid;

Chemical Property of N-(4-Chlorobenzyl)ethane-1,2-diamine

Chemical Property:

• PSA: 38.05000
• LogP: 2.47950

Purity/Quality:

≥95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-Chlorobenzyl)ethane-1,2-diamine

There total 3 articles about N-(4-Chlorobenzyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Chloro-4-(chloromethyl)benzene (104-83-6) + ethylenediamine (107-15-3,85404-18-8) → N-(4-chloro-benzyl)-ethylenediamine (53654-70-9)

Guidance literature:

In acetonitrile; at 0 - 5 ℃;

DOI:10.1021/jf803305f

Reference yield:

4-chlorobenzaldehyde (104-88-1) + ethylenediamine (107-15-3,85404-18-8) → N-(4-chloro-benzyl)-ethylenediamine (53654-70-9)

Guidance literature:

4-chlorobenzaldehyde; ethylenediamine; In methanol; Cooling with ice;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2011.08.054

Reference yield:

N,N'-bis(4-chlorobenzylidene)ethane-1,2-diamine (60434-95-9) → 1,2-bis(p-chlorobenzylamino)ethane (58015-08-0) + N-(4-chloro-benzyl)-ethylenediamine (53654-70-9)

Guidance literature:

With formic acid;

upstream raw materials:

N,N'-bis(4-chlorobenzylidene)ethane-1,2-diamine

1-Chloro-4-(chloromethyl)benzene

ethylenediamine

4-chlorobenzaldehyde

Downstream raw materials:

2-chloro-5-((2-(nitromethylene)imidazolidine-1-yl)methyl)benzene

C₂₂H₂₄ClN₅O₄

C₂₂H₂₄ClN₅O₃

C₂₃H₂₆ClN₅O₃

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