N,N-Diethyl-N'-phenylsulfuric diamide

Base Information

• Chemical Name: N,N-Diethyl-N'-phenylsulfuric diamide
• CAS No.: 53660-22-3
• Molecular Formula: C₁₀H₁₆N₂O₂S
• Molecular Weight: 228.315
• DSSTox Substance ID: DTXSID60544551
• Wikidata: Q82421685
• Mol file: 53660-22-3.mol

Synonyms:53660-22-3;N,N-Diethyl-N'-phenylsulfuric diamide;SCHEMBL10532103;DTXSID60544551;AKOS013313222

Chemical Property of N,N-Diethyl-N'-phenylsulfuric diamide

Chemical Property:

• XLogP3: 1.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 228.09324893
• Heavy Atom Count: 15
• Complexity: 262

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)S(=O)(=O)NC1=CC=CC=C1

Technology Process of N,N-Diethyl-N'-phenylsulfuric diamide

There total 3 articles about N,N-Diethyl-N'-phenylsulfuric diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diethylsulfamoyl chloride (20588-68-5) + aniline (62-53-3) → N,N-diethyl-N'-phenyl-sulfamide (53660-22-3)

Guidance literature:

DOI:10.1021/jo01063a039

Reference yield:

4-nitrophenyl N-phenylsulfamate (85599-62-8) + diethylamine (109-89-7) → N,N-diethyl-N'-phenyl-sulfamide (53660-22-3) + p-nitrophenolate (14609-74-6) + Phenyl-sulfamic acid; compound with diethyl-amine

Guidance literature:

With water; In acetonitrile; at 37 ℃; Product distribution; Rate constant; aminolysis and hydrolysis; different water:CH₃CN ratios;

DOI:10.1002/poc.610080907

Reference yield:

→ N,N-diethyl-N'-phenyl-sulfamide (53660-22-3)

Guidance literature:

Diaethylsulfamoylchlorid, PhNH2;

DOI:10.1002/9780470132395.ch29

upstream raw materials:

N,N-diethylsulfamoyl chloride

aniline

4-nitrophenyl N-phenylsulfamate

diethylamine

Refernces