N,4-diphenyl-1H-1,2,3-triazol-5-amine

Base Information

Chemical Name:N,4-diphenyl-1H-1,2,3-triazol-5-amine
CAS No.:53684-55-2
Molecular Formula:C14H12N4
Molecular Weight:236.276
Hs Code.:
European Community (EC) Number:688-681-6
DSSTox Substance ID:DTXSID40423294
Wikidata:Q82235478
ChEMBL ID:CHEMBL1345333

Synonyms:N,4-diphenyl-1H-1,2,3-triazol-5-amine;53684-55-2;N,5-diphenyl-2H-triazol-4-amine;MLS000105068;Cambridge id 5140720;Oprea1_459787;SCHEMBL2491021;CHEMBL1345333;DTXSID40423294;HMS2344E18;N,5-diphenyl-3H-triazol-4-amine;CCG-2183;AKOS003627258;SMR000054997;N,5-diphenyl-2H-1,2,3-triazol-4-amine;FT-0657999;1H-1,2,3-Triazol-5-amine, N,4-diphenyl-;AB00074348-01;A829732

Suppliers and Price of N,4-diphenyl-1H-1,2,3-triazol-5-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of N,4-diphenyl-1H-1,2,3-triazol-5-amine

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:236.106196400
Heavy Atom Count:18
Complexity:246

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NNN=C2NC3=CC=CC=C3

Technology Process of N,4-diphenyl-1H-1,2,3-triazol-5-amine

There total 7 articles about N,4-diphenyl-1H-1,2,3-triazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 29704-63-0
1,4-diphenyl-1H-1,2,3-triazol-5-amine

: 53684-55-2
N,4-diphenyl-1H-1,2,3-triazol-5-amine

Guidance literature:: With potassium tert-butylate; In neat (no solvent); at 150 - 180 ℃; for 6h; Sealed tube;
DOI:10.1002/ejoc.202001620

Reference yield:

: 140-29-4
phenylacetonitrile

: 53684-55-2
phenyl-(5-phenyl-1H-[1,2,3]triazol-4-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate

2: 184 - 185 °C

With sodium methylate;
DOI:10.1021/jo01357a018

Reference yield:

: 140-29-4
phenylacetonitrile

: 53684-55-2
N,4-diphenyl-1H-1,2,3-triazol-5-amine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / neat (no solvent) / 24 h / 25 °C / Sealed tube

2: potassium tert-butylate / neat (no solvent) / 6 h / 150 - 180 °C / Sealed tube

With potassium tert-butylate; In neat (no solvent); 2: |Dimroth Rearrangement;
DOI:10.1002/ejoc.202001620