Benzoxazole, 2-(bromomethyl)-6-(phenylmethoxy)-

Base Information

Chemical Name:Benzoxazole, 2-(bromomethyl)-6-(phenylmethoxy)-
CAS No.:536974-97-7
Molecular Formula:C15H12BrNO2
Molecular Weight:318.17
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoxazole, 2-(bromomethyl)-6-(phenylmethoxy)-

Chemical Property:

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Technology Process of Benzoxazole, 2-(bromomethyl)-6-(phenylmethoxy)-

There total 3 articles about Benzoxazole, 2-(bromomethyl)-6-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1252592-60-1
6-(benzyloxy)-2-methylbenzoxazole

: 536974-97-7
6-(benzyloxy)-2-(bromomethyl)benzoxazole

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 2h; Reflux;
DOI:10.1002/cmdc.201000203

Reference yield:

: 5078-07-9
6-hydroxy-2-methylbenzoxazole

: 536974-97-7
6-(benzyloxy)-2-(bromomethyl)benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

1.2: 20 °C

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Reflux

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/cmdc.201000203

Reference yield:

: 100-39-0
benzyl bromide

: 536974-97-7
6-(benzyloxy)-2-(bromomethyl)benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

1.2: 20 °C

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Reflux

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/cmdc.201000203