4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine

Base Information

Chemical Name:4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine
CAS No.:13616-67-6
Molecular Formula:C₁₂H₁₅NS
Molecular Weight:205.324
Hs Code.:
NSC Number:169204
DSSTox Substance ID:DTXSID10305134
Wikidata:Q82051608

Synonyms:13616-67-6;NSC169204;DTXSID10305134;NSC-169204;2-phenyl-4,5-dimethyl-3,6-dihydro-1,2-thiazine;4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine

Suppliers and Price of 4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine

Chemical Property:

Vapor Pressure:0.000927mmHg at 25°C
Boiling Point:303.5°Cat760mmHg
Flash Point:137.4°C
Density:1.078g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:205.09252066
Heavy Atom Count:14
Complexity:229

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CSN(C1)C2=CC=CC=C2)C

Technology Process of 4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine

There total 4 articles about 4,5-dimethyl-2-phenyl-3,6-dihydro-2H-1,2-thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118622-93-8
N-(phenylaminothio)phthalimide

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 13616-67-6
2-phenyl-4,5-dimethyl-3,6-dihydro-2H-1,2-thiazine

: 118623-10-2
N-phenyl-3-methyl-2-methylenebut-3-ene-1-sulphenamide

Guidance literature:: With triethylamine; In acetone; at 20 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/P19900003225

Reference yield:

: 36138-85-9
2-phenyl-but-2-enoic acid N-anilinosulfanyl-anilide

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 13616-67-6
2-phenyl-4,5-dimethyl-3,6-dihydro-2H-1,2-thiazine

Guidance literature:: In benzene; at 140 ℃; for 6h;
DOI:10.1021/jo00797a010

Reference yield:

: 3768-55-6
N-trimethylsilylaniline

: 13616-67-6
2-phenyl-4,5-dimethyl-3,6-dihydro-2H-1,2-thiazine

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 0 °C

2: 1.) Et₃N / 1.) acetone, RT_.

With triethylamine; In chloroform;
DOI:10.1039/c39880000950