Bis(4-iodophenyl)methane

Base Information

• Chemical Name: Bis(4-iodophenyl)methane
• CAS No.: 23055-78-9
• Molecular Formula: C13H10 I2
• Molecular Weight: 420.031
• NSC Number: 87363
• DSSTox Substance ID: DTXSID40293136
• Nikkaji Number: J836.541E
• Wikidata: Q82031755
• Mol file: 23055-78-9.mol

Synonyms:Bis(4-iodophenyl)methane;23055-78-9;1-iodo-4-[(4-iodophenyl)methyl]benzene;4,4'-Diiododiphenylmethane;1-iodo-4-(4-iodobenzyl)benzene;Methane, bis(p-iodophenyl)-;NSC87363;Bis(p-iodophenyl)methane;SCHEMBL5491719;DTXSID40293136;AWNHELPYJJKYDP-UHFFFAOYSA-N;Benzene,1'-methylenebis[4-iodo-;NSC-87363;AKOS024275104;AI-942/13331802

Chemical Property of Bis(4-iodophenyl)methane

Chemical Property:

• Boiling Point: 373.4°Cat760mmHg
• Flash Point: 180°C
• Density: 1.972g/cm³
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 419.88720
• Heavy Atom Count: 15
• Complexity: 157

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1CC2=CC=C(C=C2)I)I

Technology Process of Bis(4-iodophenyl)methane

There total 14 articles about Bis(4-iodophenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

ethylenediamine (107-15-3,85404-18-8) + 2,2-bis-(4-iodo-phenyl)-indan-1,3-dione (233598-98-6) → 2-(2-aminoethyl)-1H-isoindole-1,3(2H)-dione (71824-24-3) + bis(4-iodophenyl)methane (23055-78-9)

Guidance literature:

for 0.0333333h; microwave irradiation;

Reference yield: 85.0%

ethylenediamine (107-15-3,85404-18-8) + 3-[bis-(4-iodo-phenyl)-methylene]-3H-isobenzofuran-1-one (233599-02-5) → 2-(2-aminoethyl)-1H-isoindole-1,3(2H)-dione (71824-24-3) + bis(4-iodophenyl)methane (23055-78-9)

Guidance literature:

at 20 ℃; for 1h;

DOI:10.1016/j.commatsci.2005.07.004

Reference yield: 80.0%

4,4'-diamino diphenyl methane (101-77-9) → bis(4-iodophenyl)methane (23055-78-9)

Guidance literature:

4,4'-diamino diphenyl methane; With toluene-4-sulfonic acid; In water; at 20 ℃;

With potassium iodide; In water; at 20 ℃; for 2h;

DOI:10.1055/s-0030-1260046

upstream raw materials:

formaldehyd

iodobenzene

1,1,1-trichloro-2,2-di(4-iodophenyl)ethane

Diphenylmethane

Downstream raw materials:

4,4'-diiodobenzophenone

4,4'-distyryldiphenylmethane

bis(4-(phenylthio)phenyl)methane

bis<4-<(trimethylsilyl)ethynyl>phenyl>methane