Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate

Base Information

Chemical Name:Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate
CAS No.:54147-04-5
Molecular Formula:C7H11N3O2
Molecular Weight:169.183
Hs Code.:
DSSTox Substance ID:DTXSID901179526

Synonyms:Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate;54147-04-5;ethyl 5-amino-1-methylimidazole-4-carboxylate;1H-IMIDAZOLE-4-CARBOXYLIC ACID, 5-AMINO-1-METHYL-, ETHYL ESTER;Imidazole-4-carboxylic acid, 5-amino-1-methyl-, ethyl ester;Oprea1_354284;SCHEMBL1990691;DTXSID901179526;STK351133;AKOS004121054;MB02378;BS-50496;CS-0056195;FT-0754640;EN300-140811;Ethyl5-amino-1-methyl-1H-imidazole-4-carboxylate;SR-01000529570;SR-01000529570-1;Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate #;5-AMINO-1-METHYL-1H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER

Suppliers and Price of Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 10 raw suppliers

Chemical Property of Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate

Chemical Property:

Vapor Pressure:2.34E-05mmHg at 25°C
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:169.085126602
Heavy Atom Count:12
Complexity:174

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(N(C=N1)C)N

Technology Process of Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate

There total 11 articles about Ethyl 5-amino-1-methyl-1H-imidazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: ethyl 2-amino-3-cyanopropanoate

: 74-89-5
methylamine

: 54147-04-5
5-amino-1-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: ethyl 2-amino-3-cyanopropanoate; orthoformic acid triethyl ester; In acetonitrile; at 90 ℃; for 1h;

methylamine; In ethanol; acetonitrile; at 20 ℃; for 18h;

With hydrogenchloride; sodium hydrogencarbonate; more than 3 stages;

Reference yield: 37.0%

: ethyl 3-nitriloalaninate

: 122-51-0
orthoformic acid triethyl ester

: 74-89-5
methylamine

: 54147-04-5
5-amino-1-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: ethyl 3-nitriloalaninate; orthoformic acid triethyl ester; In acetonitrile; at 90 ℃; for 1h;

methylamine; In ethanol; acetonitrile; at 20 ℃; for 18h;

Reference yield:

: 122-51-0
orthoformic acid triethyl ester

: 74-89-5
methylamine

: 32683-02-6
ethyl-2-aminocyano acetate

: 54147-04-5
5-amino-1-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: With hydrogenchloride; sodium ethanolate; Yield given. Multistep reaction; 1.) acetonitrile, 90 deg C, 1 h; 2.) ethanol, 20 deg C, 5 h;