Benzenepropanoyl chloride, 4-chloro-b-(4-chlorophenyl)-

Base Information

Chemical Name:Benzenepropanoyl chloride, 4-chloro-b-(4-chlorophenyl)-
CAS No.:55010-16-7
Molecular Formula:C15H11Cl3O
Molecular Weight:313.611
Hs Code.:

Synonyms:

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanoyl chloride, 4-chloro-b-(4-chlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanoyl chloride, 4-chloro-b-(4-chlorophenyl)-

There total 5 articles about Benzenepropanoyl chloride, 4-chloro-b-(4-chlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2540-35-4
3,3-bis-(4-chloro-phenyl)-propionic acid

: 55010-16-7
3,3-bis(p-chlorophenyl)-propionic acid chloride

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 1615-02-7,940-62-5
p-chlorocinnamic acid

: 55010-16-7
3,3-bis(p-chlorophenyl)-propionic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; acetic acid / tetrahydrofuran; water / 24 h / 80 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 0 - 20 °C

With oxalyl dichloride; palladium diacetate; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/acs.orglett.1c00781

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 55010-16-7
3,3-bis(p-chlorophenyl)-propionic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; acetic acid / tetrahydrofuran; water / 24 h / 80 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 0 - 20 °C

With oxalyl dichloride; palladium diacetate; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/acs.orglett.1c00781