4-(bromomethyl)-N-phenylbenzamide

Base Information

Chemical Name:4-(bromomethyl)-N-phenylbenzamide
CAS No.:566885-74-3
Molecular Formula:C14H12BrNO
Molecular Weight:290.159
Hs Code.:
European Community (EC) Number:862-658-2
Mol file:566885-74-3.mol

Synonyms:4-(bromomethyl)-N-phenylbenzamide;566885-74-3;AKOS000118607;EN300-10788

Suppliers and Price of 4-(bromomethyl)-N-phenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

AK Scientific
4-(Bromomethyl)-N-phenylbenzamide
5g
$ 1103.00

Total 0 raw suppliers

Chemical Property of 4-(bromomethyl)-N-phenylbenzamide

Chemical Property:

Melting Point:174 - 177 °C
PSA：29.10000
LogP:3.90680
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:289.01023
Heavy Atom Count:17
Complexity:243

Purity/Quality:: 4-(Bromomethyl)-N-phenylbenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=O)C2=CC=C(C=C2)CBr

Technology Process of 4-(bromomethyl)-N-phenylbenzamide

There total 2 articles about 4-(bromomethyl)-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52780-16-2
4-bromomethylbenzoyl chloride

: 62-53-3
aniline

: 566885-74-3
N-phenyl-4-bromomethylbenzamide

Guidance literature:: With pyridine; In hexane; toluene; at 20 ℃;
DOI:10.1016/S0223-5234(03)00013-8

Reference yield:

: 6232-88-8
4-bromomethylbenzoic Acid

: 566885-74-3
N-phenyl-4-bromomethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 3 h / 0 °C

2: pyridine / toluene; hexane / 20 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In hexane; dichloromethane; toluene;
DOI:10.1016/S0223-5234(03)00013-8

Reference yield: 79.0%

: 52924-71-7
2-(prop-2-yn-1-ylsulfanyl)benzo[d]oxazole

: 566885-74-3
N-phenyl-4-bromomethylbenzamide

: 4-((4-((benzo[d]oxazol-2-ylthio)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-phenylbenzamide

Guidance literature:: With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; for 8h;
DOI:10.1007/s12039-020-01844-8