4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

Base Information

Chemical Name:4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide
CAS No.:566885-82-3
Molecular Formula:C₂₅H₂₂N₄O₃S
Molecular Weight:458.541
Hs Code.:

Synonyms:4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

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Chemical Property of 4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

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Technology Process of 4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

There total 4 articles about 4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 16699-14-2
4-methyl-N-(pyrimidin-2-yl)benzenesulfonamide

: 566885-74-3
N-phenyl-4-bromomethylbenzamide

: 566885-82-3
4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

: N-phenyl-4-{[pyrimidin-2-yl-(toluene-4-sulfonyl)-amino]-methyl}-benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/S0223-5234(03)00013-8

Reference yield:

: 6232-88-8
4-bromomethylbenzoic Acid

: 566885-82-3
4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 3 h / 0 °C

2: pyridine / toluene; hexane / 20 °C

3: 54 percent / diisopropylethylamine / dimethylformamide / 16 h / 20 °C

With pyridine; oxalyl dichloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0223-5234(03)00013-8

Reference yield:

: 52780-16-2
4-bromomethylbenzoyl chloride

: 566885-82-3
4-{[2-{[(4-methylphenyl)sulfonyl]imino}pyrimidin-1-(2H)-yl]methyl}-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / toluene; hexane / 20 °C

2: 54 percent / diisopropylethylamine / dimethylformamide / 16 h / 20 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0223-5234(03)00013-8