2-Propenoyl azide, 3-(3-nitrophenyl)-, (2E)-

Base Information

• Chemical Name: 2-Propenoyl azide, 3-(3-nitrophenyl)-, (2E)-
• CAS No.: 569348-67-0
• Molecular Formula: C9H6N4O3
• Molecular Weight: 218.172
• Mol file: 569348-67-0.mol

Synonyms:

Chemical Property of 2-Propenoyl azide, 3-(3-nitrophenyl)-, (2E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Propenoyl azide, 3-(3-nitrophenyl)-, (2E)-

There total 3 articles about 2-Propenoyl azide, 3-(3-nitrophenyl)-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(E)-3-Nitrocinnamic acid (555-68-0,1772-76-5) → 3-nitro-cinnamoyl azide (569348-67-0)

Guidance literature:

With sodium azide; N,N-dimethyl-formamide; trichlorophosphate; at 10 - 15 ℃; for 2h;

DOI:10.1081/SCC-120015815

Reference yield:

3-nitro-cinnamic acid hydrazide (91085-72-2) → 3-nitro-cinnamoyl azide (569348-67-0)

Guidance literature:

With hydrogenchloride; diethyl ether; water; sodium nitrite;

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + diethyl ether (60-29-7,927820-24-4) + (2E)-3-(3-nitrophenyl)acrylohydrazide (91085-72-2) + water (7732-18-5) → 3-nitro-cinnamoyl azide (569348-67-0)

Guidance literature:

upstream raw materials:

3-nitro-cinnamic acid hydrazide

hydrogenchloride

diethyl ether

(2E)-3-(3-nitrophenyl)acrylohydrazide

Downstream raw materials:

m-Nitrocinnamic Acid

Refernces