1-Benzoyl-1,2-dihydroquinoline

Base Information

Chemical Name:1-Benzoyl-1,2-dihydroquinoline
CAS No.:29724-68-3
Molecular Formula:C16H13 N O
Molecular Weight:235.285
Hs Code.:2933499090
NSC Number:266119
UNII:RB5J55ZG6L
DSSTox Substance ID:DTXSID10183878
Nikkaji Number:J48.331A
Wikidata:Q83054735
Mol file:29724-68-3.mol

Synonyms:1-Benzoyl-1,2-dihydroquinoline;Quinoline, 1,2-dihydro-1-benzoyl-;29724-68-3;NSC-266119;Quinoline, 1-benzoyl-1,2-dihydro-;NSC 266119;BRN 0179083;N-benzoylquinoline;NSC266119;Quinoline,2-dihydro-;RB5J55ZG6L;SCHEMBL8705933;DTXSID10183878;Phenyl-1(2H)-quinolinylmethanone;Methanone, phenyl-1(2H)-quinolinyl-

Suppliers and Price of 1-Benzoyl-1,2-dihydroquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Benzoyl-1,2-dihydroquinoline

Chemical Property:

Vapor Pressure:1.67E-06mmHg at 25°C
Boiling Point:396.8°C at 760 mmHg
Flash Point:186.5°C
PSA：20.31000
Density:1.19g/cm³
LogP:3.42520
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:235.099714038
Heavy Atom Count:18
Complexity:330

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C=CC2=CC=CC=C2N1C(=O)C3=CC=CC=C3

Technology Process of 1-Benzoyl-1,2-dihydroquinoline

There total 6 articles about 1-Benzoyl-1,2-dihydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 612-18-0
1,2-dihydroquinoline

: 98-88-4
benzoyl chloride

: 29724-68-3
1-benzoyl-1,2-dihydroquinoline

Guidance literature:: 1,2-dihydroquinoline; With pyridine; dmap; In dichloromethane; at 0 ℃; for 0.333333h;

benzoyl chloride; In dichloromethane; at 0 ℃;
DOI:10.1021/acs.orglett.0c03171

Reference yield: 72.0%

: N-(2-formylphenyl)-N-(3-methylbut-2-en-1-yl)benzamide

: 29724-68-3
1-benzoyl-1,2-dihydroquinoline

Guidance literature:: With 2,3-diazabicyclo[2.2.1]heptane bis-trifluoroacetic acid; In isopropyl alcohol; at 140 ℃; for 12h; Sealed tube;
DOI:10.1021/acs.orglett.0c02116

Reference yield:

: 91-22-5
quinoline

: 29724-68-3
1-benzoyl-1,2-dihydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

2.1: pyridine; dmap / dichloromethane / 0.33 h / 0 °C

2.2: 0 °C

With pyridine; dmap; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.0c03171