5,6-dimethoxy-1,2,3,4-tetrahydroisoquinolinium chloride

Base Information

• Chemical Name: 5,6-dimethoxy-1,2,3,4-tetrahydroisoquinolinium chloride
• CAS No.: 63905-67-9
• Molecular Formula: C₁₁H₁₅NO₂*ClH
• Molecular Weight: 229.707

Synonyms:Isoquinoline,1,2,3,4-tetrahydro-5,6-dimethoxy-, hydrochloride (9CI)

Chemical Property of 5,6-dimethoxy-1,2,3,4-tetrahydroisoquinolinium chloride

Chemical Property:

• Vapor Pressure: 0.000247mmHg at 25°C
• Boiling Point: 324.4°Cat760mmHg
• Flash Point: 128.1°C
• Density: g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6-dimethoxy-1,2,3,4-tetrahydroisoquinolinium chloride

There total 14 articles about 5,6-dimethoxy-1,2,3,4-tetrahydroisoquinolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tert-butyl 5,6-dimethoxy-3,4-dihydroisoquinoline-2(1H)-carboxylate → 5,6-dimethoxy-1,2,3,4-tetrahydro-isoquinoline hydrochloride (63905-67-9)

Guidance literature:

With hydrogenchloride; In methanol; water; at 20 ℃; for 5h;

Reference yield:

C23H30N2O4 (1429254-24-9) → 5,6-dimethoxy-1,2,3,4-tetrahydro-isoquinoline hydrochloride (63905-67-9)

Guidance literature:

With hydrogenchloride; In tert-butyl methyl ether; water; at 20 ℃; for 18h;

DOI:10.1021/jm3014103

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,3-dimethoxyphenethylamine (3213-29-4) → 5,6-dimethoxy-1,2,3,4-tetrahydro-isoquinoline hydrochloride (63905-67-9)

Guidance literature:

With water; und Erwaermen des Reaktionsprodukts mit wss. Salzsaeure;

DOI:10.1021/ja01323a035

upstream raw materials:

formaldehyd

2,3-dimethoxyphenethylamine

2,3-dimethyoxybenzaldehyde

C₂₃H₃₀N₂O₄

Downstream raw materials:

C₂₄H₂₅N₃O₄

5,6-dimethoxy-1,2,3,4-tetrahydro-isoquinoline

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