1,3-Benzodioxole-5-acetamide, N-[2-[3-methoxy-4-(phenylmethoxy)phenyl]ethyl]-

Base Information

Chemical Name:1,3-Benzodioxole-5-acetamide, N-[2-[3-methoxy-4-(phenylmethoxy)phenyl]ethyl]-
CAS No.:57906-93-1
Molecular Formula:C₂₅H₂₅NO₅
Molecular Weight:419.477
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Benzodioxole-5-acetamide, N-[2-[3-methoxy-4-(phenylmethoxy)phenyl]ethyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Benzodioxole-5-acetamide, N-[2-[3-methoxy-4-(phenylmethoxy)phenyl]ethyl]-

There total 6 articles about 1,3-Benzodioxole-5-acetamide, N-[2-[3-methoxy-4-(phenylmethoxy)phenyl]ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 57906-93-1
2-benzo[1,3]dioxol-5-yl-N-(4-benzyloxy-3-methoxy-phenethyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 4 h / Reflux

2: acetic acid; ammonium acetate / 100 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux

4: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane

With lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 100-39-0
benzyl bromide

: 57906-93-1
2-benzo[1,3]dioxol-5-yl-N-(4-benzyloxy-3-methoxy-phenethyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 4 h / Reflux

2: acetic acid; ammonium acetate / 100 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux

4: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane

With lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 57906-93-1
2-benzo[1,3]dioxol-5-yl-N-(4-benzyloxy-3-methoxy-phenethyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; ammonium acetate / 100 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux

3: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane

With lithium aluminium tetrahydride; ammonium acetate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.12.016