2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione

Base Information

Chemical Name:2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione
CAS No.:4335-61-9
Molecular Formula:C₁₇H₁₃NO₂
Molecular Weight:263.296
Hs Code.:
NSC Number:255283
DSSTox Substance ID:DTXSID101193095
Mol file:4335-61-9.mol

Synonyms:4335-61-9;(Z)-2-(3-Phenylallyl)isoindoline-1,3-dione;1H-Isoindole-1,3(2H)-dione, 2-[(2Z)-3-phenyl-2-propen-1-yl]-;NSC255283;2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione;SCHEMBL10421306;DTXSID101193095;NSC-255283;2-[(2Z)-3-Phenyl-2-propen-1-yl]-1H-isoindole-1,3(2H)-dione

Suppliers and Price of 2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione

Chemical Property:

Vapor Pressure:7.49E-08mmHg at 25°C
Boiling Point:437.4°Cat760mmHg
Flash Point:200.2°C
Density:1.259g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:263.094628657
Heavy Atom Count:20
Complexity:385

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CCN2C(=O)C3=CC=CC=C3C2=O
Isomeric SMILES:C1=CC=C(C=C1)/C=C\CN2C(=O)C3=CC=CC=C3C2=O

Technology Process of 2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione

There total 8 articles about 2-[(Z)-3-phenylprop-2-enyl]isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 17480-07-8
2-[(E)-3-phenylprop-2-enyl]-2,3-dihydro-1H-isoindole-1,3-dione

: 4335-61-9
2-[(Z)-3-phenylprop-2-enyl]-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: With benzophenone; In benzene; for 3h; Irradiation;
DOI:10.1021/jo00331a007

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 4510-34-3
(Z)-cinnamyl alcohol

: 4335-61-9
2-[(Z)-3-phenylprop-2-enyl]-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/acs.jmedchem.9b01030

Reference yield:

: 1108732-97-3
C₂₈H₂₃NO₂P⁽¹⁺⁾*I^(1-)

: 100-52-7
benzaldehyde

: 4335-61-9
2-[(Z)-3-phenylprop-2-enyl]-2,3-dihydro-1H-isoindole-1,3-dione

: 17480-07-8
2-[(E)-3-phenylprop-2-enyl]-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In toluene; for 16h; optical yield given as %de; Reflux; Inert atmosphere;
DOI:10.1080/00397910802369596